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  • ASTM E 1473 : 2009

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Standard Test Methods for Chemical Analysis of Nickel, Cobalt, and High-Temperature Alloys

    Available format(s):  Hardcopy, PDF

    Superseded date:  11-11-2014

    Language(s):  English

    Published date:  31-12-2010

    Publisher:  American Society for Testing and Materials

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    Scope - (Show below) - (Hide below)

    1.1 These test methods describe the chemical analysis of nickel, cobalt, and high-temperature alloys having chemical compositions within the following limits:

    ElementConcentration Range, %
    Aluminum0.005 to 7.00
    Beryllium0.001 to 0.05
    Boron0.001 to 1.00
    Calcium0.002 to 0.05
    Carbon0.001 to 1.10
    Chromium0.10 to 33.00
    Cobalt0.10 to 75.00
    Copper0.01 to 35.00
    Iron0.01 to 50.00
    Lead0.001 to 0.01
    Magnesium0.001 to 0.05
    Manganese0.01 to 3.0
    Molybdenum0.01 to 30.0
    Niobium (Columbium)0.01 to 6.0
    Nickel0.10 to 98.0
    Nitrogen0.001 to 0.20
    Phosphorus0.002 to 0.08
    Sulfur0.002 to 0.10
    Silicon0.01 to 5.00
    Tantalum0.005 to 1.00
    Tin0.002 to 0.10
    Titanium0.01 to 5.00
    Tungsten0.01 to 18.00
    Vanadium0.01 to 3.25
    Zinc0.001 to 0.01
    Zirconium0.01 to 2.50

    1.2 The test methods in this standard are contained in the sections indicated as follows:

    Sections
    Aluminum, Total by the 8-Quinolinol Gravimetric Method
    (0.20 % to 7.00 %)
    62 to 69
    Chromium by the Atomic Absorption Method
    (0.018 % to 1.00 %)
    100 to 109
    Chromium by the Peroxydisulfate OxidationTitration Method
    (0.10 % to 33.00 %)
    110 to 118
    Cobalt by the Ion-Exchange-Potentiometric Titration Method
    (2 % to 75 %)
    34 to 41
    Cobalt by the Nitroso-R-Salt Photometric Method
    (0.10 % to 5.0 %)
    42 to 51
    Copper by Neocuproine Photometric Method (0.010 % to 10.00 %) 52 to 61
    Iron by the Silver Reduction Titrimetric Method
    (1.0 % to 50.0 %)
    127 to 134
    Manganese by the Metaperiodate Photometric Method (0.05 % to
    2.00 %)
    8 to 17
    Molybdenum by the Ion Exchange8-Hydroxyquinoline
    Gravimetric Method (1.5 % to 30 %)
    119 to 126
    Molybdenum by the Photometric Method
    (0.01 % to 1.50 %)
    88 to 99
    Nickel by the Dimethylglyoxime Gravimetric Method
    (0.1 % to 84.0 %)
    70 to 77
    Niobium by the Ion ExchangeCupferron Gravimetric Method
    (0.5 % to 6.0 %)
    135 to 142
    Silicon by the Gravimetric Method (0.05 % to 5.00 %) 27 to 33
    Sulfur by the Combustion-Iodate Titration Method
    (0.006 % to 0.1 %)
    18 to 26
    Tantalum by the Ion ExchangePyrogallol Spectrophotometric
    Method (0.03 % to 1.0 %)
    143 to 151
    Tin by the Solvent Extraction-Atomic Absorption Method
    (0.002 % to 0.10 %)
    78 to 87

    1.3 Methods for the determination of several elements not included in these test methods can be found in Test Methods E 30, E 76, and E 1019.

    1.4 Some of the concentration ranges given in 1.1 are too broad to be covered by a single method, and therefore, these test methods contain multiple methods for some elements. The user must select the proper test method by matching the information given in the scope and interference sections of each test method with the composition of the alloy to be analyzed.

    1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E 380 are also used.

    1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7 and in 13.4, 29.1, 66.3, 123.5, 124.14, 139.4, 139.5, 147.5, and 147.6.

    8.1 This test method covers the determination of manganese in concentrations from 0.05 % to 2.00 %.

    18.1 This test method covers the determination of sulfur in concentrations from 0.006 % to 0.1 %.

    27.1 This test method covers the determination of silicon in concentrations from 0.05 % to 5.00 % in alloys containing not more than 0.1 % boron.

    34.1 This test method covers the determination of cobalt in concentrations from 2 % to 75 %.

    42.1 This test method covers the determination of cobalt in concentrations from 0.10 % to 5.0 %.

    52.1 This test method covers the determination of copper in concentrations from 0.010 % to 1.50 %.

    62.1 This test method covers the determination of total aluminum in concentrations from 0.20 % to 7.00 %.

    70.1 This test method covers the determination of nickel in concentrations from 0.1 % to 84.0 %.

    78.1 This test method covers the determination of tin in the range from 0.002 % to 0.10 %.

    88.1 This test method covers the determination of molybdenum in concentrations from 0.01 % to 1.50 %.

    100.1 This test method covers the determination of chromium in concentrations from 0.018 % to 1.00 %.

    110.1 This test method covers the determination of chromium in concentrations from 0.10 % to 33.00 %.

    119.1 This test method covers the determination of molybdenum in concentrations from 1.5 % to 30 %.

    127.1 This test method covers the determination of iron in concentrations from 1.0 % to 50.0 %.

    135.1 This test method covers the determination of niobium (columbium) in concentrations from 0.5 % to 6.0 %.

    143.1 This test method covers the determination of tantalum in concentrations from 0.03 % to 1.0 %.

    General Product Information - (Show below) - (Hide below)

    Committee E 01
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM B 637 : 2018 Standard Specification for Precipitation-Hardening and Cold Worked Nickel Alloy Bars, Forgings, and Forging Stock for Moderate or High Temperature Service
    ASTM B 690 : 2018 Standard Specification for Iron-Nickel-Chromium-Molybdenum Alloy (UNS N08367) Seamless Pipe and Tube
    ASTM B 166 : 2019 Standard Specification for Nickel-Chromium-Aluminum Alloy, Nickel-Chromium-Iron Alloys, Nickel-Chromium-Cobalt-Molybdenum Alloy, Nickel-Iron-Chromium-Tungsten Alloy, and Nickel-Chromium-Molybdenum-Copper Alloy Rod, Bar, and Wire
    ASTM B 880 : 2014 : R2019 Standard Specification for General Requirements for Chemical Check Analysis Limits for Nickel, Nickel Alloys and Cobalt Alloys
    ASTM B 865 : 2004 : R2015 Standard Specification for Precipitation Hardening Nickel-Copper-Aluminum Alloy (UNS N05500) Bar, Rod, Wire, Forgings, and Forging Stock
    ASTM B 718 : 2000 : R2016 Standard Specification for Nickel-Chromium-Molybdenum-Cobalt-Tungsten-Iron-Silicon Alloy (UNS N06333) Plate, Sheet, and Strip
    ASTM B 167 : 2018 Standard Specification for Nickel-Chromium-Aluminum Alloys (UNS N06699), Nickel-Chromium-Iron Alloys (UNS N06600, N06601, N06603, N06690, N06693, N06025, N06045, and N06696), Nickel-Chromium-Cobalt-Molybdenum Alloy (UNS N06617), Nickel-Iron-Chromium-Tungsten Alloy (UNS N06674), and Nickel-Chromium-Molybdenum-Copper Alloy (UNS N06235) Seamless Pipe and Tube
    ASTM B 474/B474M : 2019 Standard Specification for Electric Fusion Welded Nickel and Nickel Alloy Pipe
    ASTM B 688 : 2018 Standard Specification for Chromium-Nickel-Molybdenum-Iron (UNS N08367) Plate, Sheet, and Strip
    ASTM B 163 : 2018 Standard Specification for Seamless Nickel and Nickel Alloy Condenser and Heat-Exchanger Tubes
    ASTM B 815 : 2002 : R2016 Standard Specification for Cobalt-Chromium-Nickel-Molybdenum-Tungsten Alloy (UNS R31233) Rod
    ASTM B 564 : 2018 Standard Specification for Nickel Alloy Forgings
    ASTM F 3055 : 2014 : REV A Standard Specification for Additive Manufacturing Nickel Alloy (UNS N07718) with Powder Bed Fusion
    ASTM B 621 : 2002 : R2016 Standard Specification for Nickel-Iron-Chromium-Molybdenum Alloy (UNS N08320) Rod
    ASTM B 756 : 2000 : R2016 Standard Specification for Nickel-Chromium-Molybdenum-Tungsten Alloy(UNS N06110) Rod and Bar (Withdrawn 2021)
    ASTM B 775/B775M : 2019 Standard Specification for General Requirements for Nickel and Nickel Alloy Welded Pipe
    ASTM B 425 : 2011 : R2017 Standard Specification for Ni-Fe-Cr-Mo-Cu Alloy (UNS N08825, UNS N08221, and UNS N06845) Rod and Bar
    ASTM B 574 : 2018 Standard Specification for Low-Carbon Nickel-Chromium-Molybdenum, Low-Carbon Nickel-Molybdenum-Chromium, Low-Carbon Nickel-Molybdenum-Chromium-Tantalum, Low-Carbon Nickel-Chromium-Molybdenum-Copper, and Low-Carbon Nickel-Chromium-Molybdenum-Tungsten Alloy Rod
    ASTM B 691 : 2018 Standard Specification for Iron-Nickel-Chromium-Molybdenum Alloy (UNS N08367) Rod, Bar, and Wire
    ASTM B 462 : 2018 Standard Specification for Forged or Rolled Nickel Alloy Pipe Flanges, Forged Fittings, and Valves and Parts for Corrosive High-Temperature Service
    ASTM B 936 : 2019 Standard Specification for Copper-Chromium-Iron-Titanium Alloy Plate, Sheet, Strip and Rolled Bar
    ASTM B 581 : 2017 Standard Specification for Nickel-Chromium-Iron-Molybdenum-Copper Alloy Rod
    ASTM B 829 : 2019 Standard Specification for General Requirements for Nickel and Nickel Alloys Seamless Pipe and Tube
    ASTM B 573 : 2006 : R2016 Standard Specification for Nickel-Molybdenum-Chromium-Iron Alloys (UNS N10003, N10242) Rod
    ASTM B 472 : 2018 Standard Specification for Nickel Alloy Billets and Bars for Reforging
    ASTM B 751 : 2019 Standard Specification for General Requirements for Nickel and Nickel Alloy Welded Tube
    ASTM B 473 : 2007 : R2018 Standard Specification for UNS N08020, UNS N08024, and UNS N08026 Nickel Alloy Bar and Wire
    ASTM B 546 : 2004 : R2014 Standard Specification for Electric Fusion-Welded Ni-Cr-Co-Mo Alloy (UNS N06617), Ni-Fe-Cr-Si Alloys (UNS N08330 and UNS N08332), Ni-Cr-Fe-Al Alloy (UNS N06603), Ni-Cr-Fe Alloy (UNS N06025), and Ni-Cr-Fe-Si Alloy (UNS N06045) Pipe
    ASTM B 168 : 2019 Standard Specification for Nickel-Chromium-Aluminum Alloys (UNS N06699), Nickel-Chromium-Iron Alloys (UNS N06600, N06601, N06603, N06690, N06693, N06025, N06045, and N06696), Nickel-Chromium-Cobalt-Molybdenum Alloy (UNS N06617), Nickel-Iron-Chromium-Tungsten Alloy (UNS N06674), and Nickel-Chromium-Molybdenum-Copper Alloy (UNS N06235) Plate, Sheet, and Strip
    ASTM B 872 : 2006 : R2016 Standard Specification for Precipitation-Hardening Nickel Alloys Plate, Sheet, and Strip
    ASTM B 834 : 2017 Standard Specification for Pressure Consolidated Powder Metallurgy Iron-Nickel-Chromium-Molybdenum (UNS N08367), Nickel-Chromium-Molybdenum-Columbium (Nb) (UNS N06625), Nickel-Chromium-Iron Alloys (UNS N06600 and N06690), and Nickel-Chromium-Iron-Columbium-Molybdenum (UNS N07718) Alloy Pipe Flanges, Fittings, Valves, and Parts
    ASTM F 3056 : 2014 : EDT 1 Standard Specification for Additive Manufacturing Nickel Alloy (UNS N06625) with Powder Bed Fusion
    ASTM B 446 : 2019 Standard Specification for Nickel-Chromium-Molybdenum-Columbium Alloy (UNS N06625), Nickel-Chromium-Molybdenum-Silicon Alloy (UNS N06219), and Nickel-Chromium-Molybdenum-Tungsten Alloy (UNS N06650) Rod and Bar
    ASTM B 475 : 2007 : R2018 Standard Specification for UNS N08020, UNS N08024, and UNS N08026 Nickel Alloy Round Weaving Wire
    ASTM B 511/B511M : 2016 Standard Specification for Nickel-Iron-Chromium-Silicon Alloy Bars and Shapes
    ASTM B 755 : 2000 : R2016 Standard Specification for Nickel-Chromium-Molybdenum-Tungsten Alloys (UNS N06110) Plate, Sheet, and Strip (Withdrawn 2021)
    ASTM B 164 : 2003 : R2019 Standard Specification for Nickel-Copper Alloy Rod, Bar, and Wire
    ASTM B 672 : 2002 : R2018 Standard Specification for Nickel-Iron-Chromium-Molybdenum-Columbium Stabilized Alloy (UNS N08700) Bar and Wire
    ASTM B 572 : 2006 : R2016 Standard Specification for UNS N06002, UNS N06230, UNS N12160, and UNS R30556 Rod
    ASTM B 804 : 2002 : R2018 Standard Specification for UNS N08367 and UNS N08926 Welded Pipe
    ASTM F 3213 : 2017 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Cobalt-28 Chromium-6 Molybdenum via Powder Bed Fusion
    ASTM B 906 : 2019 Standard Specification for General Requirements for Flat-Rolled Nickel and Nickel Alloys Plate, Sheet, and Strip
    ASTM B 408 : 2006 : R2016 Standard Specification for Nickel-Iron-Chromium Alloy Rod and Bar
    ASTM B 649 : 2017 Standard Specification for Ni-Fe-Cr-Mo-Cu-N Low-Carbon Alloys (UNS N08925, UNS N08031, UNS N08034, UNS N08354, and UNS N08926), and Cr-Ni-Fe-N Low-Carbon Alloy (UNS R20033) Bar and Wire, and Ni-Cr-Fe-Mo-N Alloy (UNS N08936) Wire
    ASTM B 443 : 2000 : R2014 Standard Specification for Nickel-Chromium-Molybdenum-Columbium Alloy(UNS N06625) and Nickel-Chromium-Molybdenum-SiliconAlloy (UNS N06219) Plate, Sheet, and Strip
    ASTM B 805 : 2006 : R2017 : EDT 1 Standard Specification for Precipitation Hardening Nickel Alloys Bar and Wire
    ASTM B 160 : 2005 : R2019 Standard Specification for Nickel Rod and Bar
    ASTM B 335 : 2003 : R2018 Standard Specification for Nickel-Molybdenum Alloy Rod
    ASTM B 512 : 2004 : R2014 Standard Specification for Nickel-Chromium-Silicon Alloy (UNS N08330) Billets and Bars
    ASTM B 719 : 2000 : R2014 Standard Specification for Nickel-Chromium-Molybdenum-Cobalt-Tungsten-Iron-Silicon Alloy (UNS N06333) Bar
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