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ASTM E 2823 : 2017 : REDLINE

Current
Current

The latest, up-to-date edition.

Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)
Available format(s)

Hardcopy Redline , PDF Redline

Language(s)

English

Published date

01-01-2017

CONTAINED IN VOL. 03.05, 2017 Specifies the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B 02, and having chemical compositions.

1.1This test method describes the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B02, and having chemical compositions within the following limits:

Element

Application Range (Mass Fraction %)

Aluminum

0. 01–6.00

Boron

0. 01–0.10

Carbon

0. 01–0.15

Chromium

0. 01–33.00

Copper

0.01–35.00

Cobalt

0. 01–20.00

Iron

0.05–50.00

Magnesium

0. 01–0.020

Molybdenum

0. 01–30.0

Niobium

0. 01–6.0

Nickel

25.00–100.0

Phosphorous

0.001–0.025

Silicon

0.01–1.50

Sulfur

0.0001–0.01

Titanium

0.0001–6.0

Tungsten

0.01–5.0

Vanadium

0.0005–1.0

1.2The following elements may be determined using this method.

Element

Quantification Range (μg/g)

Antimony

0.5–50

Bismuth

0.1–11

Gallium

2.9–54

Lead

0.4–21

Silver

1–35

Tin

2.2–97

Thallium

0.5–3.0

1.3This method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this method to other elements or different composition ranges provided that method validation that includes evaluation of method sensitivity, precision, and bias as described in this document is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user is cautioned to carefully evaluate the validation data as to the intended purpose of the analytical results. Guide E2857 provides additional guidance on method validation.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.

Committee
E 01
DocumentType
Redline
Pages
10
PublisherName
American Society for Testing and Materials
Status
Current

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ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 50 : 2017 : REDLINE Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 2165 : 2001 Standard Practice for Establishing an Uncertainty Budget for the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2007)
ASTM E 1479 : 2016 : REDLINE Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 2972 : 2015 Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 1601 : 2012 : REDLINE Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)

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