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ASTM E 2866 : 2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

01-02-2012

CONTAINED IN VOL. 15.08, 2017 Defines the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil.

1.1 This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). OPs are qualitatively and quantitatively determined by this method.

1.2 UnitsThe values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 The Method Detection Limit (MDL), electrospray ionization (ESI) mode and Reporting Range for the OPs are listed in Table 1.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

TABLE 1 Method Detection Limit and Reporting Range

AnalyteESI
Mode
MDL
(PPB)
Reporting Range
(PPB)
Diisopropyl methylphosphonatePositive2.740-2000
Ethyl methylphosphonic acidNegative2.340-2000
Ethyl methylphosphonic acidPositive1.340-2000
Isopropyl methylphosphonic acidNegative5.740-2000
Isopropyl methylphosphonic acidPositive2.840-2000
Methylphosphonic acidPositive8.740-2000
Pinacolyl methylphosphonic acidNegative5.340-2000

Committee
E 54
DocumentType
Test Method
Pages
15
ProductNote
Reconfirmed 2012
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

ASTM E 2771 : 2011 : R2019 Standard Terminology for Homeland Security Applications

CFR 40(PTS100-149) : JUL 94 PROTECTION OF ENVIRONMENT - ENVIRONMENTAL PROTECTION AGENCY
ASTM D 3740 : 2012-06 PRACTICE FOR MINIMUM REQUIREMENTS FOR AGENCIES ENGAGED IN TESTING AND/OR INSPECTION OF SOIL AND ROCK AS USED IN ENGINEERING DESIGN AND CONSTRUCTION
ASTM E 2554 : 2013-05 PRACTICE FOR ESTIMATING AND MONITORING THE UNCERTAINTY OF TEST RESULTS OF A TEST METHOD USING CONTROL CHART TECHNIQUES
ASTM D 653 : 2014 : REDLINE Standard Terminology Relating to Soil, Rock, and Contained Fluids

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