Name: ASTM E 2866 : 2021
Brand: ASTM
Price: 57.60 GBP

Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid, and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography/Tandem Mass Spectrometry

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

10-05-2021

Publisher

American Society for Testing and Materials

1.1This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA), and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). OPs are qualitatively and quantitatively determined by this method.

1.2Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3The method detection limit2 (MDL), electrospray ionization (ESI) mode, and reporting range3 for the OPs are listed in Table 1.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee	D 34
DocumentType	Test Method
Pages	15
PublisherName	American Society for Testing and Materials
Status	Current
Supersedes	ASTM E 2866 : 2012 : R2016

ASTM E 2771 : 2011 : R2019

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