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  • ASTM E 3047 : 2016

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    Standard Test Method for Analysis of Nickel Alloys by Spark Atomic Emission Spectrometry

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  12-05-2016

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 03.05, 2016 Specifies the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B 02, having chemical compositions.

    Scope - (Show below) - (Hide below)

    1.1This method describes the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B02, having chemical compositions within the following limits:

    Element

    Application Range (Mass Fraction, %)

    Aluminum

    0.005-6.00

    Boron

    0.001-0.10

    Carbon

    0.005-0.15

    Chromium

    0.01-33.00

    Copper

    0.01-35.00

    Cobalt

    0.01-25.00

    Iron

    0.05-55.00

    Magnesium

    0.001-0.020

    Manganese

    0.01-1.00

    Molybdenum

    0.01-35.00

    Niobium

    0.01-6.0

    Nickel

    25.00-100.0

    Phosphorous

    0.001-0.025

    Silicon

    0.01-1.50

    Sulfur

    0.0001-0.01

    Titanium

    0.0001-6.0

    Tantalum

    0.01-0.15

    Tin

    0.001-0.020

    Tungsten

    0.01-5.0

    Vanadium

    0.0005-1.0

    Zirconium

    0.01-0.10

    1.2The following elements may be determined using this method.

    Element

    Quantification Range (Mass Fraction, %)

    Aluminum

    0.010-1.50

    Boron

    0.004-0.025

    Carbon

    0.014-0.15

    Chromium

    0.09-20.0

    Cobalt

    0.05-14.00

    Copper

    0.03-0.6

    Iron

    0.17-20

    Magnesium

    0.001-0.03

    Manganese

    0.04-0.6

    Molybdenum

    0.07-5.0

    Niobium

    0.02-5.5

    Phosphorous

    0.005-0.020

    Silicon

    0.07-0.6

    Sulfur

    0.002-0.005

    Tantalum

    0.025-0.15

    Tin

    0.001-0.02

    Titanium

    0.025-3.2

    Tungsten

    0.02-0.10

    Vanadium

    0.005-0.25

    Zirconium

    0.01-0.05

    1.3This method has been interlaboratory tested for the elements and quantification ranges specified in section 1.2. The ranges in section 1.2 indicate intervals within which results have been demonstrated to be quantitative. It may be possible to extend this method to other elements or different composition ranges provided that a method validation study as described in Guide E2857 is performed and that the results of this study show that the method extension is meeting laboratory data quality objectives. Supplemental data on other elements not included in the scope are found in the supplemental data tables of the Precision and Bias section.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.

    General Product Information - (Show below) - (Hide below)

    Committee E 01
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    SAE AMS 7001 : 2018 NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, POWDER FOR ADDITIVE MANUFACTURING, 62NI - 21.5CR - 9.0MO - 3.65NB
    SAE AMS 7000 : 2018 LASER-POWDER BED FUSION (L-PBF) PRODUCED PARTS, NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, 62NI - 21.5CR - 9.0MO - 3.65NB STRESS RELIEVED, HOT ISOSTATIC PRESSED AND SOLUTION ANNEALED

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM E 1257 : 2016 Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
    ASTM E 2857 : 2021 Standard Guide for Validating Analytical Methods
    ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 1257 : 1993 : R1998 : EDT 1 Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
    ASTM E 1329 : 2000 : R2005 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 1601 : 2019 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 1601 : 1998 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 2972 : 2015 Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
    ASTM E 1601 : 2010 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 1329 : 2010 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
    ASTM E 1329 : 2000 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
    ASTM E 1601 : 2012 : REDLINE Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 305 : 2013 Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 305 : 2013 : REDLINE Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves
    ASTM E 1601 : 2012 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 2857 : 2011 : R2021 : EDT 1 Standard Guide for Validating Analytical Methods
    ASTM E 1257 : 1993 : R2003 Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 2857 : 2011 : R2016 Standard Guide for Validating Analytical Methods
    ASTM E2972 : 2015(2019) Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
    ASTM E 135 : 2021 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 305 : 2021 Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves
    ASTM E 2857 : 2011 Standard Guide for Validating Analytical Methods
    ASTM E 1257 : 1993 : R2008 Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
    ASTM E 135 : 2020 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
    ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM E 1257 : 2016 : REDLINE Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
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