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BS EN 14105:2011

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of free and total glycerol and mono-, di-, triglyceride contents
Available format(s)

Hardcopy , PDF

Superseded date

11-12-2020

Language(s)

English

Published date

31-05-2011

Foreword
1 Scope
2 Principle
3 Reagents
4 Apparatus
5 Preparation of solutions
6 Sampling
7 Procedure
8 Determination of results
9 Expression of results
10 Precision
11 Test report
Annex A (informative) - Sample chromatogram
Annex B (normative) - Calibration function calculation
Annex C (informative) - Worked example
Annex D (informative) - Results of the interlaboratory
        trial
Bibliography

Describes a method to determine the free glycerol and residual mono-, di-, and triglyceride contents in fatty acid methyl esters (FAME) intended for addition to mineral oils.

The purpose of this European Standard is to determine the free glycerol and residual mono-, di- and triglyceride contents in fatty acid methyl esters (FAME) intended for addition to mineral oils. The total glycerol content is then calculated from the obtained results.

Under the conditions described, the quantification limits are 0,001 % (m/m) for free glycerol, 0,10 % (m/m) for all glycerides (mono-, di- and tri-). This method is suitable for FAME prepared from rapeseed, sunflower, soybean, palm, animal oils and fats and mixture of them. It is not suitable for FAME produced from or containing coconut and palm kernel oils derivatives because of overlapping of different glyceride peaks.

NOTE For the purposes of this European Standard, the term “% (m/m)?? is used to represent respectively the mass fraction.

WARNING — The use of this method may involve hazardous equipment, materials and operations. This method does not purport to address to all of the safety problems associated with its use, but it is the responsibility of the user to search and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
AW/307
DevelopmentNote
Supersedes 01/707544 DC (05/2003) Supersedes 09/30207063 DC. (05/2011)
DocumentType
Standard
Pages
26
PublisherName
British Standards Institution
Status
Superseded
SupersededBy
Supersedes

Standards Relationship
ONORM EN 14105 : 2011 Identical
UNE-EN 14105:2003 Identical
DIN EN 14105:2011-07 Identical
NF EN 14105 : 2011 Identical
I.S. EN 14105:2011 Identical
NEN EN 14105 : 2011 Identical
NS EN 14105 : 2011 Identical
EN 14105:2011 Identical
UNI EN 14105 : 2011 Identical
NBN EN 14105 : 2011 Identical
SN EN 14105 : 2011 Identical

ISO 5555:2001 Animal and vegetable fats and oils — Sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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