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BS ISO 11709:2011

Current
Current

The latest, up-to-date edition.

Soil quality. Determination of selected coal-tar-derived phenolic compounds using high performance liquid chromatography (HPLC)
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-05-2011

Publisher

British Standards Institution

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Reagents
7 Apparatus
8 Sampling and preservation of samples
9 Procedure
10 Calculation and expression of results
11 Test report
Annex A (informative) - Example of chromatographic conditions
        and chromatogram
Annex B (informative) - Emission spectrum (FLD, 280 nm to
        900 nm) recorded with FLD Agilent 1100
Annex C (informative) - Ultraviolet spectrum (DAD, 200 nm to
        350 nm), recorded with Dionex UVD 320S
Annex D (informative) - Examples of limits of determinations
        of coal-tar-derived phenols for different HPLC detectors
Bibliography

Describes a method for the quantitative determination of selected coal-tar-derived phenols, namely phenol, methylphenols such as (ortho-, meta-, para-)cresols, and dihydroxybenzenes such as catechol, resorcinol and hydroquinone in soil by using high performance liquid chromatography with ultraviolet/diode array (HPLC/UV/DAD) or fluorescence (HPLC/FLD) or electrochemical detection (HPLC/ELCD).

This International Standard specifies a method for the quantitative determination of selected coal-tar-derived phenols, namely phenol, methylphenols such as (ortho-, meta-, para-)cresols, and dihydroxybenzenes such as catechol, resorcinol and hydroquinone (see Table1) in soil by using high performance liquid chromatography with ultraviolet/diode array (HPLC/UV/DAD) or fluorescence (HPLC/FLD) or electrochemical detection (HPLC/ELCD). It is applicable to all types of soil with contamination levels of individual phenols in the range of approximately 0,08mg/kg to 10mg/kg of soil.

NOTE Also with this method, other higher methylated phenols, for example, dimethylphenols such as (2,3-, 2,4-, 2,5-, 2,6-, 3,4- and 3,5-)xylenoles, 2-isopropylphenol, 2,3,5-trimethylphenol and 1-naphthol can be analysed, provided the suitability and the validity of the method are proven.

Committee
EH/4
DocumentType
Standard
Pages
30
PublisherName
British Standards Institution
Status
Current

Standards Relationship
ISO 11709:2011 Identical

ISO 16072:2002 Soil quality Laboratory methods for determination of microbial soil respiration
ISO 10381-1:2002 Soil quality Sampling Part 1: Guidance on the design of sampling programmes
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 648:2008 Laboratory glassware — Single-volume pipettes
ISO 10381-2:2002 Soil quality Sampling Part 2: Guidance on sampling techniques
DIN 32645:2008-11 CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
ISO 14154:2005 Soil quality — Determination of some selected chlorophenols — Gas-chromatographic method with electron-capture detection

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Hardcopy - English
PDF - English
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