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BS ISO 17947:2014

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of fine silicon nitride powders
Available format(s)

Hardcopy , PDF

Withdrawn date

11-04-2023

Language(s)

English

Published date

31-08-2014

Foreword
Introduction
1 Scope
2 Normative references
3 Analytes and ranges
4 Preparation of test sample
5 Apparatus and reagents
6 Blank test
7 Determination of total silicon
8 Determination of total nitrogen
9 Determination of aluminium, iron, and calcium
10 Determination of oxygen
11 Determination of carbon
12 Determination of fluorine and chlorine
13 Reporting analytical values
14 Test report
Annex A (informative) - List of commercial certified
        reference materials
Annex B (informative) - Analytical results obtained
        from a round robin test
Annex C (informative) - Spectral lines for ICP-OES
Bibliography

Defines the methods for the chemical analysis of fine silicon nitride powders used as the raw material for fine ceramics.

This International Standard specifies the methods for the chemical analysis of fine silicon nitride powders used as the raw material for fine ceramics.

This International Standard stipulates the determination methods of total silicon, total nitrogen, aluminium, iron, calcium, oxygen, carbon, fluorine, and chlorine in fine silicon nitride powders.

Committee
RPI/13
DevelopmentNote
Supersedes 13/30261099 DC. (09/2014)
DocumentType
Standard
Pages
44
PublisherName
British Standards Institution
Status
Withdrawn
Supersedes

Standards Relationship
ISO 17947:2014 Identical

ISO 6353-1:1982 Reagents for chemical analysis — Part 1: General test methods
EN 12698-1:2007 Chemical analysis of nitride bonded silicon carbide refractories - Part 1: Chemical methods
ISO 21438-2:2009 Workplace atmospheres — Determination of inorganic acids by ion chromatography — Part 2: Volatile acids, except hydrofluoric acid (hydrochloric acid, hydrobromic acid and nitric acid)
ISO 21438-3:2010 Workplace atmospheres — Determination of inorganic acids by ion chromatography — Part 3: Hydrofluoric acid and particulate fluorides
ISO 2828:1973 Aluminium oxide primarily used for the production of aluminium — Determination of fluorine content — Alizarin complexone and lanthanum chloride spectrophotometric method
ISO 21068-2:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 2: Determination of loss on ignition, total carbon, free carbon and silicon carbide, total and free silica and total and free silicon
ISO 6353-3:1987 Reagents for chemical analysis — Part 3: Specifications — Second series
ENV 14226:2002 Advanced technical ceramics - Test methods for ceramic powders - Determination of calcium, magnesium, iron and aluminium in silicon nitride by using flame atomic absorption spectroscopy (FAAS) or inductively coupled plasma atomic emission spectroscopy (ICP-AES)
EN 12698-2:2007 Chemical analysis of nitride bonded silicon carbide refractories - Part 2: XRD methods
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 21068-3:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 3: Determination of nitrogen, oxygen and metallic and oxidic constituents
ISO 26845:2008 Chemical analysis of refractories General requirements for wet chemical analysis, atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods
ISO 8656-1:1988 Refractory products Sampling of raw materials and unshaped products Part 1: Sampling scheme

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