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CAN/CSA-Z5100-17

Current
Current

The latest, up-to-date edition.

Cellulose nanomaterials - Test methods for characterization
Available format(s)

PDF , Hardcopy

Language(s)

French, English

Published date

01-01-2017

Preface
0 Introduction
1 Scope
2 Reference publications
3 Definitions
4 General
5 Test methods for characterization
Annex A (informative) - Dispersion
Annex B (informative) - Modification and compatibilization
Annex C (informative) - Inclusion of CNMs in nano-enhanced
        and nano-enabled products
Annex D (informative) - Commercial product life-cycle
Annex E (informative) - Environment, health, and safety (EHS)
Annex F (informative) - Commercial product requirements
Annex G (informative) - Sustainability
Annex H (informative) - Bibliography

Specifies test methods for characterization of base cellulose nanomaterials, specifically those designated as cellulose nanocrystals (CNCs), cellulose nanofibrils (CNFs) and cellulose microfibrils (CMFs).

Preface This is the second edition of CSA Z5100, Cellulose nanomaterials — Test methods for characterization. It supersedes the first edition, published in 2014. The major differences between this edition and the previous edition include: a) addition of a new test method for CMF content (consistency); b) addition of more information on recommended test methods for degree of crystallinity, colour and ISO brightness, and morphology; c) updated test methods for viscosity and rheological properties, total sulfur content, sulfate half- ester content, carboxylate content, thermal stability, and dispersibility in aqueous media; and d) alignment with new CSA standard Z5200. This Standard provides a consolidated set of test methods to characterize base cellulose nanomaterials. This Standard is the first in a series on cellulose nanomaterials intended to serve as a foundation for the development of both Canadian and international standards to facilitate introduction of cellulose nanomaterials into global markets. This is a companion standard to CSA Z5200. Cellulose nanomaterials extracted from cellulose sources, such as wood pulps, are biodegradable, sustainable, and retain the non-toxicity of cellulose. These materials have numerous potential applications in areas such as composite materials, optical films and devices, catalysts, and pharmaceuticals. Scope 1.1 This Standard describes test methods for characterization of base cellulose nanomaterials, specifically those designated as cellulose nanocrystals (CNCs), cellulose nanofibrils (CNFs) and cellulose microfibrils (CMFs). Note: These designations, particularly CNFs and CMFs, are not used consistently among cellulose nanomaterial producers and users; therefore there is some overlap as to which materials fall under which designation. 1.2 This Standard does not cover the characterization of cellulose microcrystals (CMCs). 1.3 This Standard does not cover cellulose nanomaterial-based nano-enhanced or nano-enabled products. Note: This Standard might be expanded in future editions as cellulose nanomaterial-enhanced and -enabled products move towards commercialization. See Annex C. 1.4 In this Standard, \"shall\" is used to express a requirement, i.e., a provision that the user is obliged to satisfy in order to comply with the standard; \"should\" is used to express a recommendation or that which is advised but not required; and \"may\" is used to express an option or that which is permissible within the limits of the standard. Notes accompanying clauses do not include requirements or alternative requirements; the purpose of a note accompanying a clause is to separate from the text explanatory or informative material. Notes to tables and figures are considered part of the table or figure and may be written as requirements. Annexes are designated normative (mandatory) or informative (non-mandatory) to define their application. 1.5 The values given in SI units are the units of record for the purposes of this Standard. The values given in parentheses are for information and comparison only.

DevelopmentNote
Also available in CSA Z5100/Z5200 PACKAGE. (06/2017) French Edition issued on 01-11-2017. ERRATA 2018 is only available in French Version. (03/2018)
DocumentType
Standard
ISBN
978-1-4883-0825-3
Pages
0
PublisherName
Canadian Standards Association
Status
Current
Supersedes

CAN/CSA-Z5200-17 Cellulose nanomaterials - Blank detail specification
ISO/TR 19716:2016 Nanotechnologies Characterization of cellulose nanocrystals
PD ISO/TR 19716:2016 Nanotechnologies. Characterization of cellulose nanocrystals
CSA Z5100/Z5200 PACKAGE : 2017 CONSISTS OF Z5100-17, CELLULOSE NANOMATERIALS - TEST METHODS FOR CHARACTERIZATION AND Z5200-17, CELLULOSE NANOMATERIALS - BLANK DETAIL SPECIFICATION

ISO 22412:2017 Particle size analysis — Dynamic light scattering (DLS)
TAPPI T 236 : 2013 KAPPA NUMBER OF PULP
ISO 4094:2005 Paper, board and pulps International calibration of testing apparatus Nomination and acceptance of standardizing and authorized laboratories
ISO 2884-2:2003 Paints and varnishes — Determination of viscosity using rotary viscometers — Part 2: Disc or ball viscometer operated at a specified speed
ISO 6588-1:2012 Paper, board and pulps Determination of pH of aqueous extracts Part 1: Cold extraction
ISO 9276-1:1998 Representation of results of particle size analysis — Part 1: Graphical representation
ISO 5631-1:2015 Paper and board — Determination of colour by diffuse reflectance — Part 1: Indoor daylight conditions (C/2 degrees)
ISO 13099-1:2012 Colloidal systems — Methods for zeta-potential determination — Part 1: Electroacoustic and electrokinetic phenomena
TAPPI T 204 : 2007 SOLVENT EXTRACTIVES OF WOOD AND PULP
ISO 29301:2010 Microbeam analysis Analytical transmission electron microscopy Methods for calibrating image magnification by using reference materials having periodic structures
ISO 302:2015 Pulps Determination of Kappa number
ISO 638:2008 Paper, board and pulps Determination of dry matter content Oven-drying method
ISO/TR 13097:2013 Guidelines for the characterization of dispersion stability
TAPPI T 249 : 1985 CARBOHYDRATE COMPOSITION OF EXTRACTIVE-FREE WOOD AND WOOD PULP BY GAS-LIQUID CHROMATOGRAPHY
ISO 187:1990 Paper, board and pulps — Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples
ISO 5263-3:2004 Pulps — Laboratory wet disintegration — Part 3: Disintegration of mechanical pulps at > 85 degrees C
ISO 1628-3:2010 Plastics Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 3: Polyethylenes and polypropylenes
ISO 12830:2011 Paper, board and pulps Determination of acid-soluble magnesium, calcium, manganese, iron, copper, sodium and potassium
ISO Guide 82:2014 Guidelines for addressing sustainability in standards
ISO 2470-1:2016 Paper, board and pulps Measurement of diffuse blue reflectance factor Part 1: Indoor daylight conditions (ISO brightness)
TAPPI T 648 : 2014 VISCOSITY OF COATING CLAY SLURRY
ISO 13322-1:2014 Particle size analysis — Image analysis methods — Part 1: Static image analysis methods
CAN/CSA-Z5200-17 Cellulose nanomaterials - Blank detail specification
ISO 14644-1:2015 Cleanrooms and associated controlled environments Part 1: Classification of air cleanliness by particle concentration
ISO 7027-1:2016 Water quality Determination of turbidity Part 1: Quantitative methods
ISO/TS 80004-1:2015 Nanotechnologies — Vocabulary — Part 1: Core terms
ISO/TR 3666:1998 Viscosity of water
ISO 20998-1:2006 Measurement and characterization of particles by acoustic methods Part 1: Concepts and procedures in ultrasonic attenuation spectroscopy
ISO 2469:2014 Paper, board and pulps — Measurement of diffuse radiance factor (diffuse reflectance factor)
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
TAPPI T 262 : 2012 PREPARATION OF MECHANICAL PULPS FOR TESTING
TAPPI T 230 : 2013 VISCOSITY OF PULP (CAPILLARY VISCOMETER METHOD)
ISO 11952:2014 Surface chemical analysis Scanning-probe microscopy Determination of geometric quantities using SPM: Calibration of measuring systems
ISO 5351:2010 Pulps Determination of limiting viscosity number in cupri-ethylenediamine (CED) solution
ISO 3105:1994 Glass capillary kinematic viscometers — Specifications and operating instructions
ISO/TS 80004-4:2011 Nanotechnologies — Vocabulary — Part 4: Nanostructured materials
ISO 12058-1:1997 Plastics Determination of viscosity using a falling-ball viscometer Part 1: Inclined-tube method
TAPPI T 205 : 2006 FORMING HANDSHEETS FOR PHYSICAL TESTS OF PULP
ISO 9277:2010 Determination of the specific surface area of solids by gas adsorption — BET method
ISO 13099-2:2012 Colloidal systems — Methods for zeta-potential determination — Part 2: Optical methods
ISO 14488:2007 Particulate materials — Sampling and sample splitting for the determination of particulate properties
ISO 4119:1995 Pulps Determination of stock concentration
ISO/TS 80004-2:2015 Nanotechnologies — Vocabulary — Part 2: Nano-objects

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