CEN/TS 14429:2005

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Characterization of waste - Leaching behaviour tests - Influence of pH on leaching with initial acid/base addition

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Withdrawn date: 07-03-2023

Language(s):

Published date: 19-10-2005

Publisher: Comite Europeen de Normalisation

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Table of Contents - (Show below) - (Hide below)

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle
6 Reagents and laboratory devices
   6.1 Reagents
   6.2 Laboratory devices
7 Sampling
   7.1 Laboratory sample
   7.2 Preparation of test sample
   7.3 Determination of dry residue
   7.4 Test portion
8 Test procedure
   8.1 Contact time
   8.2 pH-range
   8.3 Leaching test
   8.4 Natural pH
9 Eluate treatment, storage and analysis
10 Blank test
11 Performance characteristics
12 Test report
Annex A (informative) - Example of a data sheet
Annex B (informative) - Operation and uses of the test:
        influence of pH on the leaching behaviour
Annex C (informative) - Preliminary determination of the
        acid/base consumption
Annex D (informative) - Examples of acid and base neutralisation
        capacities for waste, soil, sediment and construction
        materials
Bibliography

Abstract - (Show below) - (Hide below)

This Technical Specification is applicable to determine the influence of pH on the leachability of inorganic constituents from a waste material. Equilibrium condition as defined in the standard is established by addition of pre-determined amounts of acid or base to reach desired end pH values. This test method produces eluates, which are subsequently characterized physically and chemically. This Technical Specification is a parameter specific test as specified in ENV 12920. The application of this test method alone is not sufficient for the determination of the detailed leaching behaviour of a waste under specified conditions.NOTEThis generally requires the application of several test methods, behavioural modelling and model validation as specified in ENV 12920.

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Committee	CEN/TC 292
Document Type	Technical Specification
ISBN
Pages
Published
Publisher	Comite Europeen de Normalisation
Status	Withdrawn
Superseded By	EN 14429:2015

National Adoptions - (Show below) - (Hide below)

Equivalent Standard(s)	Relationship
DIN CEN/TS 14429:2006-01	Identical
XP CEN/TS 14429 : 2006 XP	Identical
UNI CEN/TS 14429 : 2006	Identical
I.S. CEN TS 14429:2005	Identical
DD CEN/TS 14429:2005 (published 2006-02)	Identical
NEN NPR CEN/TS 14429 : 2005	Identical

Standards Referenced By This Book - (Show below) - (Hide below)

06/30156589 DC : DRAFT OCT 2006	ISO 21268-4 - SOIL QUALITY LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
PD CEN/TR 16376:2012	Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
DD CEN/TS 14997:2006 (published 2006-12)	Characterization of waste. Leaching behaviour tests. Influence of pH on leaching with continuous pH-control
UNI CEN ISO/TS 21268-4 : 2010	SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
I.S. CEN TS 14997:2006	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - INFLUENCE OF PH ON LEACHING WITH CONTINUOUS PH-CONTROL
CEN/TS 15862:2012	Characterisation of waste - Compliance leaching test - One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
CEN/TR 16376:2012	Characterization of waste - Overall guidance document for characterization of waste from the extractive industries
EN 15875:2011/AC:2012	CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
CEN/TS 15364:2006	Characterization of waste - Leaching behaviour tests - Acid and base neutralization capacity test
CEN ISO/TS 21268-4:2009	Soil quality - Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials - Part 4: Influence of pH on leaching with initial acid/base addition (ISO/TS 21268-4:2007)
DIN EN ISO 18772 E : 2014	SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
10/30233988 DC : 0	BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
18/30368510 DC : 0	BS EN ISO 21268-4 - SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
UNI EN ISO 18772 : 2014	SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
DIN EN ISO 18772:2014-07	Soil quality - Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials (ISO 18772:2008)
S.R. CEN/TR 16376:2012	CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
S.R. CEN/TS 15863:2012	CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERISATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
S.R. CEN/TS 15862:2012	CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
BS EN 16192:2011	Characterization of waste. Analysis of eluates
BS EN 15875:2011 (published 2013-04)	Characterisation of waste. Static test for determination of acid potential and neutralisation potential of sulfidic waste
DIN EN 16192:2012-02	Characterization of waste - Analysis of eluates
BS EN ISO 18772:2014	Soil quality. Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
DD CEN/TS 15364:2006 (published 2006-07)	Characterization of waste. Leaching behaviour tests. Acid and base neutralization capacity test
S.R. CEN/TR 16110:2010	CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
I.S. EN 16192:2011	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
UNI CEN/TS 15862 : 2012	CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
DIN EN 15875 E : 2012	CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
I.S. CEN TS 15364:2006	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - ACID AND BASE NEUTRALIZATION CAPACITY TEST
I.S. EN 15875:2011	CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
DIN EN 15875:2012-11	Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste (includes Corrigendum :2012)
12/30263896 DC : 0	BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
UNI EN 15875 : 2011	CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
FD CEN/TR 16110 : 2011 FD	CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
PD CEN/TS 15862:2012	Characterisation of waste. Compliance leaching test. One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
PD CEN/TS 15863:2012	Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions
ISO 18772:2008	Soil quality — Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
ISO/TS 21268-4:2007	Soil quality Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials Part 4: Influence of pH on leaching with initial acid/base addition
EN ISO 18772:2014	Soil quality - Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials (ISO 18772:2008)
S.R. CEN ISO TS 21268-4:2009	SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
UNE-EN 15875:2012	Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste
08/30189276 DC : 0	BS EN 15875 - CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL OF SULFIDIC WASTE
UNE-EN 16192:2012	Characterization of waste - Analysis of eluates
UNE-CEN/TR 16110:2011 IN	Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
BS ISO 18772 : 2008 COR 2014	SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
I.S. EN ISO 18772:2014	SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
UNI EN 16192 : 2012	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
CEN/TS 14997 : 2006	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - INFLUENCE OF PH ON LEACHING WITH CONTINUOUS PH-CONTROL
CEN/TR 16110:2010	Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
EN 16192:2011	Characterization of waste - Analysis of eluates
CEN/TS 15863:2012	Characterisation of waste - Leaching behaviour test for basic characterisation - Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions

Standards Referencing This Book - (Show below) - (Hide below)

PREN 14346 : DRAFT 2004	CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE AND WATER CONTENT
ENV 12920 : 1997	CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
EN 13370:2003	Characterization of waste - Analysis of eluates - Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN-, F-
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
EN 12506:2003	Characterization of waste - Analysis of eluates - Determination of pH, As, Ba, Cd, Cl-, Co, Cr, Cr Vl, Cu, Mo, Ni, NO2-, Pb, total S, SO42-, V and Zn
PREN 14997 : DRAFT 2013	CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - INFLUENCE OF PH ON LEACHING WITH CONTINUOUS PH CONTROL

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