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CEN/TS 16183:2012

Current
Current

The latest, up-to-date edition.

Sludge, treated biowaste and soil - Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC-MS)
Published date

22-02-2012

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample storage
8 Procedure
9 Calibration
10 Calculation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Repeatability and reproducibility
        data
Annex B (informative) - Example of a reference solution for
        multipoint calibration
Annex C (informative) - Examples for gas chromatographic
        conditions
Annex D (informative) - Flow scheme of the determination
        of phthalates
Bibliography

This Technical Specification specifies a method for the determination of selected phthalates in sludge, treated biowaste and soil, after extraction and gas chromatographic analysis with mass spectrometric detection.The method is applicable for the determination of phthalates (see Table 2) at the lowest mass content of 0,1 mg/kg to 0,5 mg/kg (expressed as dry matter), depending on the individual substance. The applicability of the method to other phthalates not specified in Table 2 is not excluded except the isomeric mixtures e.g. DiNP (Di-isononylphthalate), but shall be verified in each case.

Committee
CEN/TC 444
DocumentType
Technical Specification
PublisherName
Comite Europeen de Normalisation
Status
Current

16/30340580 DC : 0 BS EN 17009 - FLOORING OF LIGNIFIED MATERIALS OTHER THAN WOOD - CHARACTERISTICS, EVALUATION OF CONFORMITY AND MARKING

ISO 5667-13:2011 Water quality Sampling Part 13: Guidance on sampling of sludges
PREN 15934 : DRAFT 2009 SOIL, SLUDGE, WASTE, AND TREATED BIOWASTE - DETERMINATION OF DRY MATTER - GRAVIMETRIC METHOD
ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 383:1976 Laboratory glassware — Interchangeable conical ground joints
PREN 16179 : DRAFT 2010 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
ISO 10381-2:2002 Soil quality Sampling Part 2: Guidance on sampling techniques
ISO 5667-15:2009 Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 5667-13:2011 Water quality - Sampling - Part 13: Guidance on sampling of sludges (ISO 5667-13:2011)
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN ISO 5667-15:2009 Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009)

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