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  • DIN EN 15309 E : 2007

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    CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2007

    Publisher:  German Institute for Standardisation (Deutsches Institut für Normung)

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Safety remarks
    5 Principle
    6 Apparatus
    7 Reagents
    8 Interferences and sources of error
    9 Sample preparation
       9.1 General
       9.2 Drying and determination of dry mass
       9.3 Preparation of pressed pellet
       9.4 Preparation of fused beads
    10 Procedure
       10.1 Analytical measurement conditions
       10.2 Calibration
       10.3 Analysis of the samples
    11 Quality control
       11.1 Drift correction procedure
       11.2 Blank test
       11.3 Reference materials
    12 Calculation of the result
    13 Test report
    Annex A (informative) Semi-quantitative screening analysis
                          of waste, sludge and soil samples
    Annex B (informative) Examples for operational steps of
                          the sample preparation for soil and
                          waste samples
    Annex C (informative) Suggested analytical lines, crystals and
                          operating conditions
    Annex D (informative) List of reference materials applicable
                          for XRF-analysis
    Annex E (informative) Validation
    Bibliography
    National Annex (informative) Bibliography

    Abstract - (Show below) - (Hide below)

    Gives the procedure for a quantitative determination of major and trace element concentrations in homogeneous solid waste, soil and soil-like material by energy dispersive X-ray fluorescence (EDXRF) spectrometry or wavelength dispersive X-ray fluorescence (WDXRF) spectrometry using a calibration with matrix-matched standards.

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher German Institute for Standardisation (Deutsches Institut für Normung)
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    DIN EN ISO 13196 E : 2015 SOIL QUALITY - SCREENING SOILS FOR SELECTED ELEMENTS BY ENERGY-DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY USING A HANDHELD OR PORTABLE INSTRUMENT (ISO 13196:2013)

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    ISO Guide 32:1997 Calibration in analytical chemistry and use of certified reference materials
    DIN ISO 12980 E : 2006 CARBONACEOUS MATERIALS USED IN THE PRODUCTION OF ALUMINIUM - GREEN COKE AND CALCINED COKE FOR ELECTRODES - ANALYSIS USING AN X-RAY FLUORESCENCE METHOD
    DIN 51418-2:2015-03 X-RAY SPECTROMETRY - X-RAY EMISSION AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 2: DEFINITIONS AND BASIC PRINCIPLES FOR MEASUREMENTS, CALIBRATION AND EVALUATION OF RESULTS
    ISO 12980:2000 Carbonaceous materials used in the production of aluminium — Green coke and calcined coke for electrodes — Analysis using an X-ray fluorescence method
    DIN ISO 5725-2:2002-12 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
    DIN 51418-1:2008-08 X-RAY SPECTROMETRY - X-RAY EMISSION- AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 1: DEFINITIONS AND BASIC PRINCIPLES
    ISO 12677:2011 Chemical analysis of refractory products by X-ray fluorescence (XRF) Fused cast-bead method
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    DIN ISO 11464 E : 2006 SOIL QUALITY - PRETREATMENT OF SAMPLES FOR PHYSICO-CHEMICAL ANALYSES
    ISO Guide 33:2015 Reference materials Good practice in using reference materials
    EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
    CEN/TR 15018 : 2005 CHARACTERIZATION OF WASTE - DIGESTION OF WASTE SAMPLES USING ALKALI-FUSION TECHNIQUES
    ISO 14869-2:2002 Soil quality Dissolution for the determination of total element content Part 2: Dissolution by alkaline fusion
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 13656 : 2002 CHARACTERIZATION OF WASTE - MICROWAVE ASSISTED DIGESTION WITH HYDROFLUORIC (HF), NITRIC (HNO[3]), AND HYDROCHLORIC (HCL) ACID MIXTURE FOR SUBSEQUENT DETERMINATION OF ELEMENTS
    EN ISO 12677:2011 CHEMICAL ANALYSIS OF REFRACTORY PRODUCTS BY X-RAY FLUORESCENCE (XRF) - FUSED CAST-BEAD METHOD (ISO 12677:2011)
    EN 13657 : 2002 CHARACTERIZATION OF WASTE - DIGESTION FOR SUBSEQUENT DETERMINATION OF AQUA REGIA SOLUBLE PORTION OF ELEMENTS
    ISO 9516-1:2003 Iron ores Determination of various elements by X-ray fluorescence spectrometry Part 1: Comprehensive procedure
    DIN ISO 11465:1996-12 SOIL QUALITY - DETERMINATION OF DRY MATTER AND WATER CONTENT ON A MASS BASIS - GRAVIMETRIC METHOD
    ISO Guide 34:2009 General requirements for the competence of reference material producers
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