CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2007

Publisher

German Institute for Standardisation (Deutsches Institut für Normung)

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Safety remarks
5 Principle
6 Apparatus
7 Reagents
8 Interferences and sources of error
9 Sample preparation
   9.1 General
   9.2 Drying and determination of dry mass
   9.3 Preparation of pressed pellet
   9.4 Preparation of fused beads
10 Procedure
   10.1 Analytical measurement conditions
   10.2 Calibration
   10.3 Analysis of the samples
11 Quality control
   11.1 Drift correction procedure
   11.2 Blank test
   11.3 Reference materials
12 Calculation of the result
13 Test report
Annex A (informative) Semi-quantitative screening analysis
                      of waste, sludge and soil samples
Annex B (informative) Examples for operational steps of
                      the sample preparation for soil and
                      waste samples
Annex C (informative) Suggested analytical lines, crystals and
                      operating conditions
Annex D (informative) List of reference materials applicable
                      for XRF-analysis
Annex E (informative) Validation
Bibliography
National Annex (informative) Bibliography

Gives the procedure for a quantitative determination of major and trace element concentrations in homogeneous solid waste, soil and soil-like material by energy dispersive X-ray fluorescence (EDXRF) spectrometry or wavelength dispersive X-ray fluorescence (WDXRF) spectrometry using a calibration with matrix-matched standards.

DocumentType	Standard
Pages	43
PublisherName	German Institute for Standardisation (Deutsches Institut für Normung)
Status	Current

Standards	Relationship
EN 15309:2007	Identical

DIN EN ISO 13196 E : 2015

SOIL QUALITY - SCREENING SOILS FOR SELECTED ELEMENTS BY ENERGY-DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY USING A HANDHELD OR PORTABLE INSTRUMENT (ISO 13196:2013)

ISO/IEC 17025:2005	General requirements for the competence of testing and calibration laboratories
ISO Guide 32:1997	Calibration in analytical chemistry and use of certified reference materials
DIN ISO 12980 E : 2006	CARBONACEOUS MATERIALS USED IN THE PRODUCTION OF ALUMINIUM - GREEN COKE AND CALCINED COKE FOR ELECTRODES - ANALYSIS USING AN X-RAY FLUORESCENCE METHOD
DIN 51418-2:2015-03	X-RAY SPECTROMETRY - X-RAY EMISSION AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 2: DEFINITIONS AND BASIC PRINCIPLES FOR MEASUREMENTS, CALIBRATION AND EVALUATION OF RESULTS
ISO 12980:2000	Carbonaceous materials used in the production of aluminium — Green coke and calcined coke for electrodes — Analysis using an X-ray fluorescence method
DIN ISO 5725-2:2002-12	Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
DIN 51418-1:2008-08	X-RAY SPECTROMETRY - X-RAY EMISSION- AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 1: DEFINITIONS AND BASIC PRINCIPLES
ISO 12677:2011	Chemical analysis of refractory products by X-ray fluorescence (XRF) Fused cast-bead method
ISO 11464:2006	Soil quality Pretreatment of samples for physico-chemical analysis
DIN ISO 11464 E : 2006	SOIL QUALITY - PRETREATMENT OF SAMPLES FOR PHYSICO-CHEMICAL ANALYSES
ISO Guide 33:2015	Reference materials Good practice in using reference materials
EN 14346:2006	CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
CEN/TR 15018:2005	Characterization of waste - Digestion of waste samples using alkali-fusion techniques
ISO 14869-2:2002	Soil quality Dissolution for the determination of total element content Part 2: Dissolution by alkaline fusion
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN 15002:2015	Characterization of waste - Preparation of test portions from the laboratory sample
EN 13656 : 2002	CHARACTERIZATION OF WASTE - MICROWAVE ASSISTED DIGESTION WITH HYDROFLUORIC (HF), NITRIC (HNO[3]), AND HYDROCHLORIC (HCL) ACID MIXTURE FOR SUBSEQUENT DETERMINATION OF ELEMENTS
EN ISO 12677:2011	Chemical analysis of refractory products by X-ray fluorescence (XRF) - Fused cast-bead method (ISO 12677:2011)
EN 13657:2002	Characterization of waste - Digestion for subsequent determination of aqua regia soluble portion of elements
ISO 9516-1:2003	Iron ores Determination of various elements by X-ray fluorescence spectrometry Part 1: Comprehensive procedure
DIN ISO 11465:1996-12	SOIL QUALITY - DETERMINATION OF DRY MATTER AND WATER CONTENT ON A MASS BASIS - GRAVIMETRIC METHOD
ISO Guide 34:2009	General requirements for the competence of reference material producers

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DIN EN 15309 E : 2007

Current

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