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DIN EN 15527:2008-09

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
Available format(s)

Hardcopy , PDF

Superseded date

29-07-2022

Language(s)

English, German

Published date

01-09-2008

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
   5.1 General
   5.2 Reagents for extraction procedures
   5.3 Reagents for clean-up procedures
   5.4 Reagents for gas chromatographic analysis
   5.5 Standards
6 Apparatus
   6.1 Extraction and clean-up procedures
   6.2 Gas chromatograph
   6.3 Capillary columns
   6.4 Preparation of standard solutions
7 Hazards
8 Interference
   8.1 Interference during sampling, storage and extraction
   8.2 Interference due to co-elution
9 Sample conservation
10 Pretreatment
   10.1 General
   10.2 Drying
   10.3 Particle size reduction
11 Procedure
   11.1 Blank
   11.2 Extraction
   11.3 Addition of the internal standard solution
   11.4 Concentration or dilution
   11.5 Clean up of the extract
   11.6 Addition of the injection standard
   11.7 Gas chromatographic analysis with mass
        spectrometric detection
12 Performance characteristics
13 Test report
Annex A (informative) Representative chromatograms
Annex B (informative) Additional validation data
Annex C (informative) Summary of general requirements
        and recommendations
Bibliography
National Annex NA (informative) Bibliography

Describes the quantitative determination of 16 polynuclear aromatic hydrocarbons (PAH) according to the priority list of the Environmental Protection Agency (EPA, 1982).

DocumentType
Standard
Pages
39
PublisherName
German Institute for Standardisation (Deutsches Institut für Normung)
Status
Superseded
SupersededBy

Standards Relationship
EN 15527:2008 Identical

ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 18287:2006 Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS)
DIN ISO 18287:2006-05 Soil quality - Determination of polycyclic aromatic hydrocarbons (PAH) - Gas chromatographic method with mass spectrometric detection (GC-MS) (ISO 18287:2006)
DIN ISO 14507:2004-07 SOIL QUALITY - PRETREATMENT OF SAMPLES FOR DETERMINATION OF ORGANIC CONTAMINANTS
EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
DIN ISO 22892:2006-09 SOIL QUALITY - GUIDELINES FOR THE IDENTIFICATION OF TARGET COMPOUNDS BY GAS CHROMATOGRAPHY AND MASS SPECTROMETRY
ISO 16720:2005 Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
EN ISO 16720:2007 Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample

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