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  • DIN EN 15527 E : 2008

    Current The latest, up-to-date edition.
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    CHARACTERIZATION OF WASTE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WASTE USING GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC/MS)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2008

    Publisher:  German Institute for Standardisation (Deutsches Institut für Normung)

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
       5.1 General
       5.2 Reagents for extraction procedures
       5.3 Reagents for clean-up procedures
       5.4 Reagents for gas chromatographic analysis
       5.5 Standards
    6 Apparatus
       6.1 Extraction and clean-up procedures
       6.2 Gas chromatograph
       6.3 Capillary columns
       6.4 Preparation of standard solutions
    7 Hazards
    8 Interference
       8.1 Interference during sampling, storage and extraction
       8.2 Interference due to co-elution
    9 Sample conservation
    10 Pretreatment
       10.1 General
       10.2 Drying
       10.3 Particle size reduction
    11 Procedure
       11.1 Blank
       11.2 Extraction
       11.3 Addition of the internal standard solution
       11.4 Concentration or dilution
       11.5 Clean up of the extract
       11.6 Addition of the injection standard
       11.7 Gas chromatographic analysis with mass
            spectrometric detection
    12 Performance characteristics
    13 Test report
    Annex A (informative) Representative chromatograms
    Annex B (informative) Additional validation data
    Annex C (informative) Summary of general requirements
            and recommendations
    Bibliography
    National Annex NA (informative) Bibliography

    Abstract - (Show below) - (Hide below)

    Describes the quantitative determination of 16 polynuclear aromatic hydrocarbons (PAH) according to the priority list of the Environmental Protection Agency (EPA, 1982).

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    Document Type Standard
    Publisher German Institute for Standardisation (Deutsches Institut für Normung)
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    ISO 18287:2006 Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS)
    EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
    DIN ISO 22892:2006-09 SOIL QUALITY - GUIDELINES FOR THE IDENTIFICATION OF TARGET COMPOUNDS BY GAS CHROMATOGRAPHY AND MASS SPECTROMETRY
    ISO 16720:2005 Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
    EN ISO 16720 : 2007 SOIL QUALITY - PRETREATMENT OF SAMPLES BY FREEZE-DRYING FOR SUBSEQUENT ANALYSIS
    ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
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