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EN 12607-2:2014

Current

Current

The latest, up-to-date edition.

Bitumen and bituminous binders - Determination of the resistance to hardening under influence of heat and air - Part 2: TFOT method

Published date

05-11-2014

Foreword
1 Scope
2 Normative references
3 Principle
4 Apparatus
5 Sampling
6 Procedure
7 Calculation
8 Expression of results
9 Precision
10 Test report
Annex A (informative) - Characteristics of thermometers
Bibliography

This part of EN 12607 specifies a method for measuring the combined effects of heat and air on a film of bitumen or bituminous binder, simulating the hardening which most bituminous binders undergo during mixing in an asphalt mixing plant. The method is suitable for other bituminous binders than paving grade bitumen, but the reference temperature might give excessive hardening that does not resemble real conditions during mixing at the plant. The method may not represent the hardening that occurs during mixing of warm mix binders.Additionally, this part of EN 12607 specifies a method for the determination of the change in mass of oxidized bitumens and hard industrial bitumens after heating. The method is used to detect volatile components.The method is referred to as TFOT, i.e. Thin Film Oven Test.WARNING: Use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to identify the hazards and assess the risks involved in performing this test method and to implement sufficient control measures to protect individual operators (and the environment). This includes appropriate safety and health practices and determination of the applicability of regulatory limitations prior to use.If there is a likelihood of volatile components being present in a binder, this procedure should not be used. It should not be used for cut-back bitumen or bituminous emulsions before these products have been stabilized, e.g. in accordance with EN 13074 2.

Committee
CEN/TC 336
DevelopmentNote
Supersedes PREN 12607-2. (11/2014)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

PREN 13398 : DRAFT 2016 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE ELASTIC RECOVERY OF MODIFIED BITUMEN
05/30138353 DC : DRAFT AUG 2005 EN 15323 - BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY THE ROTATING CYLINDER METHOD (RCAT)
BS EN 13398:2017 Bitumen and bituminous binders. Determination of the elastic recovery of modified bitumen
13/30273898 DC : 0 BS EN 12594 - BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
DIN EN 14769:2012-08 Bitumen and bituminous binders - Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV)
BS EN 12594:2014 Bitumen and bituminous binders. Preparation of test samples
BS EN 15323:2007 Bitumen and bituminous binders. Accelerated long-term ageing/conditioning by the rotating cylinder method (RCAT)
BS EN 12591:2009 Bitumen and bituminous binders. Specifications for paving grade bitumens
EN 12595:2014 Bitumen and bituminous binders - Determination of kinematic viscosity
EN 13303:2017 Bitumen and bituminous binders - Determination of the loss in mass after heating of industrial bitumen
05/30138279 DC : DRAFT AUG 2005 EN 12594 - BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
BS 2000-506(2009) : 2009 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE LOSS IN MASS AFTER HEATING OF INDUSTRIAL BITUMEN
BS 2000-535(2012) : 2012 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY A PRESSURE AGEING VESSEL (PAV)
EN 13398:2017 Bitumen and bituminous binders - Determination of the elastic recovery of modified bitumen
DIN EN 15323 E : 2007 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING/CONDITIONING BY THE ROTATING CYLINDER METHOD (RCAT)
UNE-EN 14769:2012 Bitumen and bituminous binders - Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV)
I.S. EN 12591:2009 BITUMEN AND BITUMINOUS BINDERS - SPECIFICATIONS FOR PAVING GRADE BITUMENS
I.S. EN 14769:2012 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY A PRESSURE AGEING VESSEL (PAV)
I.S. EN 12594:2014 BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
I.S. EN 13303:2017 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE LOSS IN MASS AFTER HEATING OF INDUSTRIAL BITUMEN
DIN EN 12591:2009-08 BITUMEN AND BITUMINOUS BINDERS - SPECIFICATIONS FOR PAVING GRADE BITUMENS
I.S. EN 12595:2014 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF KINEMATIC VISCOSITY
03/314554 DC : DRAFT OCT 2003 EN 14769 - BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING - PRESSURE AGEING VESSEL (PAV)
I.S. EN 13398:2017 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE ELASTIC RECOVERY OF MODIFIED BITUMEN
EN 12594:2014 (edition 2) Bitumen and bituminous binders - Preparation of test samples
DIN EN 12594:2015-01 BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
DIN EN 14769 E : 2012 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY A PRESSURE AGEING VESSEL (PAV)
BS EN 14769:2012 Bitumen and bituminous binders. Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV)
BS EN 12595:2014 Bitumen and bituminous binders. Determination of kinematic viscosity
UNI EN 14769 : 2013 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY A PRESSURE AGEING VESSEL (PAV)
UNI EN 12594 : 2015 BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
UNI EN 12595 : 2015 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF KINEMATIC VISCOSITY
UNI EN 12591 : 2009 BITUMEN AND BITUMINOUS BINDERS - SPECIFICATIONS FOR PAVING GRADE BITUMENS
IP 551 : 2007 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING/CONDITIONING BY THE ROTATING CYLINDER METHOD (RCAT)
DIN EN 12595:2015-01 Bitumen and bituminous binders - Determination of kinematic viscosity
DIN EN 15323:2007-07 Bitumen and bituminous binders - Accelerated long-term ageing/conditioning by the rotating cylinder method (RCAT)
BS EN 13303:2017 Bitumen and bituminous binders. Determination of the loss in mass after heating of industrial bitumen
UNE-EN 12595:2015 Bitumen and bituminous binders - Determination of kinematic viscosity
UNE-EN 12594:2015 Bitumen and bituminous binders - Preparation of test samples
IP 461 : 2007 BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
EN 14769:2012 Bitumen and bituminous binders - Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV)
EN 15323:2007 Bitumen and bituminous binders - Accelerated long-term ageing/conditioning by the rotating cylinder method (RCAT)
BS 2000-461(2000) : 2000 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
BS 2000-506(2017) : 2017 BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE LOSS IN MASS AFTER HEATING OF INDUSTRIAL BITUMEN
16/30326278 DC : 0 BS EN 13398 - BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE ELASTIC RECOVERY OF MODIFIED BITUMEN
16/30326272 DC : 0 BS EN 13303 - BITUMEN AND BITUMINOUS BINDERS - DETERMINATION OF THE LOSS IN MASS AFTER HEATING OF INDUSTRIAL BITUMEN
PREN 12591 : DRAFT 2016 BITUMEN AND BITUMINOUS BINDERS - SPECIFICATIONS FOR PAVING GRADE BITUMENS
BS 2000-551(2007) : 2007 BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING/CONDITIONING BY THE ROTATING CYLINDER METHOD (RCAT)
BS 2000-535(2005) : 2005 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - BITUMEN AND BITUMINOUS BINDERS - ACCELERATED LONG-TERM AGEING CONDITIONING BY A PRESSURE AGEING VESSEL (PAV)
PREN 12594 : DRAFT 2013 BITUMEN AND BITUMINOUS BINDERS - PREPARATION OF TEST SAMPLES
EN 12591:2009 Bitumen and bituminous binders - Specifications for paving grade bitumens

EN 1426:2015 Bitumen and bituminous binders - Determination of needle penetration
EN 1425:2012 Bitumen and bituminous binders - Characterization of perceptible properties
EN 1427:2015 Bitumen and bituminous binders - Determination of the softening point - Ring and Ball method
ASTM D 1754 : 1997 Standard Test Method for Effect of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
EN 13304:2009 Bitumen and bituminous binders - Framework for specification of oxidised bitumens
EN 58:2012 Bitumen and bituminous binders - Sampling bituminous binders
EN 13305:2009 Bitumen and bituminous binders - Framework for specification of hard industrial bitumens
EN 12594:2014 (edition 2) Bitumen and bituminous binders - Preparation of test samples
EN 13074-2:2011 Bitumen and bituminous binders - Recovery of binder from bituminous emulsion or cut-back or fluxed bituminous binders - Part 2: Stabilisation after recovery by evaporation
EN 12595:2014 Bitumen and bituminous binders - Determination of kinematic viscosity

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