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  • EN 12766-1:2000

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    Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)

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    Published date:  22-03-2000

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents and materials
    6 Apparatus
    7 Sampling and sample preparation
    8 Clean-up procedure
    9 Gaschromatographic operating conditions
    10 Check on instrumental performance
    11 Calibration
    12 Determination
    13 Calculation
    14 Expression of results
    15 Precision
    16 Test report
    Annex A (normative) Identification PCB peaks
    Annex B (normative) Alternative and additional clean-up
            procedures
    Annex C (informative) Systematic numbering of PCB compounds
    Annex D (informative) Tradenames and manufacturers
    Annex E (informative) Determination of TCBTs

    Abstract - (Show below) - (Hide below)

    This European Standard specifies a method to determine the concentration of up to 12 individual or defined unresolved small groups of polychlorinated biphenyl (PCB) congeners in petroleum products and related materials by means of a specified gaschromatographic separation procedure. The gas chromatographic separation is valid for the different quantification procedures described in Part 2 of this European Standard.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 19
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    05/30136951 DC : 0 EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE, SOIL AND SLUDGE BY USING CAPILLARY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    05/30133366 DC : DRAFT MAY 2005 EN 5XXXX BTTF 116-1 - STANDARD FOR THE INVENTORY, CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    BS EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    BS 2000-462.3(2004) : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    BS EN 1948-4 : 2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    DIN EN 1948-4:2014-03 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    06/30159746 DC : 0 BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    I.S. EN 1948-4:2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    BS EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    10/30147454 DC : 0 BS EN 16167 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    15/30330799 DC : 0 BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    12/30231385 DC : 0 BS ISO 13876 - SOIL QUALITY - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    01/124547 DC : DRAFT JAN 2002 PREN 12766-3 - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    CLC/TR 50503 : 2010 Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs
    S.R. CLC/TR 50503:2010 GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    PREN 15308 : DRAFT 2015 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    PREN 12766-3 : DRAFT 2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
    17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    UNI EN 1948-4 : 2014 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    BS 2000-462.2(2001) : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    UNE-EN 15308:2017 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    I.S. EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    ISO 13876:2013 Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    I.S. EN 12766-2:2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    I.S. EN 12766-3:2005 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    DIN EN 12766-3:2005-02 Petroleum products and used oils - Determination of PCBs and related products - Part 3: Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
    BS EN 12766-3 : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    BS EN 12766-2 : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    EN 1948-4:2010+A1:2013 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    EN 12766-2 : 2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    EN 12766-3:2004/AC:2007 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids Automatic pipeline sampling
    ISO 3170:2004 Petroleum liquids Manual sampling
    ISO 3696:1987 Water for analytical laboratory use Specification and test methods
    EN ISO 3696 : 1995 WATER FOR ANALYTICAL LABORATORY USE - SPECIFICATION AND TEST METHODS (ISO 3696:1987)
    EN ISO 3170 : 2004 PETROLEUM LIQUIDS - MANUAL SAMPLING (ISO 3170:2004)
    EN ISO 3171 : 1999 PETROLEUM LIQUIDS - AUTOMATIC PIPELINE SAMPLING
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