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  • EN 13656 : 2002

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    CHARACTERIZATION OF WASTE - MICROWAVE ASSISTED DIGESTION WITH HYDROFLUORIC (HF), NITRIC (HNO[3]), AND HYDROCHLORIC (HCL) ACID MIXTURE FOR SUBSEQUENT DETERMINATION OF ELEMENTS

    Available format(s): 

    Superseded date:  18-11-2020

    Language(s): 

    Published date:  12-01-2013

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Safety remarks
    5 Sample
       5.1 Sample pre-treatment
       5.2 Mass of test portion
    6 Equipment
       6.1 Closed vessel system
           6.1.1 Microwave unit
           6.1.2 Digestion vessels
       6.2 Semi-open vessel system
           6.2.1 Microwave unit
           6.2.2 Digestion vessels
       6.3 General equipment
    7 Reagents
    8 Interferences and sources of error
       8.1 General informations
       8.2 Closed vessel system
       8.3 Semi-open vessel system
    9 Procedure
       9.1 Blank test
       9.2 Procedure for closed vessels
           9.2.1 Amount of samples and reagents
           9.2.2 Digestion
           9.2.3 Complexation of HF
           9.2.4 Preparation of the solution for analysis
       9.3 Procedure for semi-open vessels
           9.3.1 Amount of samples
           9.3.2 Digestion and complexation of HF
           9.3.3 Preparation of the solution for analysis
    10 Test report
    Annex A (normative) Calibration of the powder adjustment
    Annex B (informative) Validation
    Bibliography

    Abstract - (Show below) - (Hide below)

    Gives methods of microwave assisted digestion with hydrofluoric (HF), nitric (HNO[3]) and hydrochloric (HCL) acid mixture. Solutions produced by the methods are suitable for analysis e.g. by atomic absorption spectrometry (FLAAS, HGAAS, CVAAS, GFAAS), inductively coupled plasma emission spectrometry (ICP-OES) and inductive coupled plasma mass spectrometry (ICP-MS).

    General Product Information - (Show below) - (Hide below)

    Committee TC 292
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By

    Standards Referenced By This Book - (Show below) - (Hide below)

    CLC/TS 50625-3-1 : 2015 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL
    DIN EN 16424 E : 2015 CHARACTERIZATION OF WASTE - SCREENING METHODS FOR THE ELEMENT COMPOSITION BY PORTABLE X-RAY FLUORESCENCE INSTRUMENTS
    DIN EN 15309:2007-08 Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence
    BS EN 15309:2007 Characterization of waste and soil. Determination of elemental composition by X-ray fluorescence
    UNI EN 15410 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    13/30272291 DC : 0 BS ISO 18227 - SOIL QUALITY - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    ISO 18227:2014 Soil quality Determination of elemental composition by X-ray fluorescence
    15/30288430 DC : 0 BS ISO 14869-3 - SOIL QUALITY - DISSOLUTION FOR THE DETERMINATION OF TOTAL ELEMENT CONTENT - PART 3: DISSOLUTION WITH HYDROFLUORIC, HYDROCHLORIC AND NITRIC ACIDS USING PRESSURISED MICROWAVE TECHNIQUE
    10/30213000 DC : 0 BS EN 15410 - SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    DIN EN 15410:2011-11 Solid recovered fuels - Method for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    DIN EN 16424:2015-03 CHARACTERIZATION OF WASTE - SCREENING METHODS FOR THE ELEMENT COMPOSITION BY PORTABLE X-RAY FLUORESCENCE INSTRUMENTS
    BS EN 15410:2011 (published 2011-09) Solid recovered fuels. Methods for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    DD CEN/TS 15410 : 2006 SOLID RECOVERED FUELS - METHOD FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    UNE-EN 15410:2012 Solid recovered fuels - Methods for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    ISO 14869-3:2017 Soil quality — Dissolution for the determination of total element content — Part 3: Dissolution with hydrofluoric, hydrochloric and nitric acids using pressurised microwave technique
    BS EN 15411:2011 (published 2011-09) Solid recovered fuels. Methods for the determination of the content of trace elements (As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Tl, V and Zn)
    UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    DIN EN 15309 E : 2007 CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    S.R. CLC/TS 50625-3-1:2015 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL
    04/30116791 DC : DRAFT JUL 2004 BS EN 15002 - CHARACTERISATION OF WASTE - PREPARATION OF TEST PORTIONS FROM LABORATORY SAMPLE
    10/30213003 DC : 0 BS EN 15411 - SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. EN 15410:2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    DD CEN/TS 15411 : 2006 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    BS ISO 14869-3:2017 Soil quality. Dissolution for the determination of total element content Dissolution with hydrofluoric, hydrochloric and nitric acids using pressurised microwave technique
    12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    NF EN 15411 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    BS EN 16424:2014 (published 2015-11) Characterization of waste. Screening methods for the element composition by portable X-ray fluorescence instruments
    BS ISO 18227 : 2014 SOIL QUALITY - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    BS PD CLC/TS 50625-3-1 : 2015 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL
    BS EN 16457:2014 (published 2014-03) Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
    BS PD CLC/TS 50625-3-3 : 2017 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAYS
    CLC/TS 50625-3-3 : 2017 Collection, logistics & treatment requirements for WEEE - Part 3-3: Specification for de-pollution - WEEE containing CRTs and flat panel displays
    NF EN 15410 : 2011 SOLID RECOVERED FUELS - METHOD FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    UNE-EN 16424:2015 Characterization of waste - Screening methods for the element composition by portable X-ray fluorescence instruments
    I.S. EN 16424:2014&LC:2014 CHARACTERIZATION OF WASTE - SCREENING METHODS FOR THE ELEMENT COMPOSITION BY PORTABLE X-RAY FLUORESCENCE INSTRUMENTS
    DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    UNI EN 15411 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    S.R. CEN/TR 16176:2011 CHARACTERIZATION OF WASTE - SCREENING METHODS FOR ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE SPECTROMETRY FOR ON-SITE VERIFICATION
    I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. CEN TS 15411:2006 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    UNE-EN 15411:2012 Solid recovered fuels - Methods for the determination of the content of trace elements (As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Tl, V and Zn)
    CEI CLC/TS 50625-3-3 : 1ED 2018 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAY
    S.R. CLC/TS 50625-3-3:2017 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAYS
    DIN EN 15411:2011-11 Solid recovered fuels - Methods for the determination of the content of trace elements (As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Tl, V and Zn)
    I.S. EN 15411:2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    I.S. CEN TS 15410:2006 SOLID RECOVERED FUELS - METHOD FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    I.S. EN 15309:2007 CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    17/30348303 DC : 0 BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
    UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    BS EN 15002:2015 (published 2015-04) Characterization of waste. Preparation of test portions from the laboratory sample
    13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 15410 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    EN 15411 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    CEN/TS 15410 : 2006 SOLID RECOVERED FUELS - METHOD FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    CEN/TS 15411 : 2006 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF TRACE ELEMENTS (AS, BA, BE, CD, CO, CR, CU, HG, MO, MN, NI, PB, SB, SE, TL, V AND ZN)
    CEN/TR 16176 : 2011 CHARACTERIZATION OF WASTE - SCREENING METHODS FOR ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE SPECTROMETRY FOR ON-SITE VERIFICATION
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 15309:2007 Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence
    EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results Part 1: General principles and definitions
    ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
    EN 1483 : 2007 WATER QUALITY - DETERMINATION OF MERCURY - METHOD USING ATOMIC ABSORPTION SPECTROMETRY
    EN ISO 5961 : 1995 WATER QUALITY - DETERMINATION OF CADMIUM BY ATOMIC ABSORPTION SPECTROMETRY (ISO 5961:1994)
    ISO 5961:1994 Water quality Determination of cadmium by atomic absorption spectrometry
    ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results Part 3: Intermediate measures of the precision of a standard measurement method
    ENV 12506 : DRAFT 2000 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, CD, CR (6), CU, NI, PB, ZN, CL[-], NO[2][-], SO[4][2-]
    ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
    ISO 8288:1986 Water quality — Determination of cobalt, nickel, copper, zinc, cadmium and lead — Flame atomic absorption spectrometric methods
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
    EN 1233 : 1996 WATER QUALITY - DETERMINATION OF CHROMIUM - ATOMIC ABSORPTION SPECTROMETRIC METHODS
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    EN ISO 3696 : 1995 WATER FOR ANALYTICAL LABORATORY USE - SPECIFICATION AND TEST METHODS (ISO 3696:1987)
    EN ISO 11969:1996 WATER QUALITY - DETERMINATION OF ARSENIC - ATOMIC ABSORPTION SPECTROMETRIC METHOD (HYDRIDE TECHNIQUE)
    ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
    EN 45001 : 1989 GENERAL CRITERIA FOR THE OPERATION OF TESTING LABORATORIES
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