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  • EN 13657 : 2002

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    CHARACTERIZATION OF WASTE - DIGESTION FOR SUBSEQUENT DETERMINATION OF AQUA REGIA SOLUBLE PORTION OF ELEMENTS

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    Language(s): 

    Published date:  16-10-2002

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Safety remarks
    5 Sample
       5.1 Sample pre-treatment
       5.2 Mass of test portion
    6 Equipment
       6.1 Closed vessel system
           6.1.1 Microwave unit
           6.1.2 Digestion vessels
       6.2 Semi-open vessel system
           6.2.1 Microwave unit
           6.2.2 Digestion vessels
       6.3 Apparatus for thermal heating digestion
           6.3.1 Reaction vessels
           6.3.2 Reflux condenser
           6.3.3 Absorption vessel
           6.3.4 Roughened glass beards
           6.3.5 Temperature-controlled heating apparatus
       6.4 General equipment
    7 Reagents
    8 Interferences and sources of error
       8.1 General informations
       8.2 Closed vessel system
       8.3 Semi-open vessel system for microwave or thermal
           heating digestion
    9 Procedure
       9.1 Blank test
       9.2 Procedure for microwave assisted digestion in closed
           vessels
       9.3 Procedure for microwave assisted digestion in semi-open
           vessels
           9.3.1 Amount of samples
           9.3.2 Digestion
           9.3.3 Preparation of the solution for analysis
       9.4 Procedure for thermal heating digestion in reflux systems
           9.4.1 Amount of samples
           9.4.2 Digestion
           9.4.3 Preparation of the solution for analysis
    10 Test report
    Annex A (normative) Calibration of the power adjustment
    Annex B (informative) Validation
          B.1 Inter-laboratory study
          B.2 Robustness study
    Bibliography

    Abstract - (Show below) - (Hide below)

    This standard specifies methods of digestion with aqua regia.

    General Product Information - (Show below) - (Hide below)

    Committee TC 444
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    S.R. CLC/TS 50625-3-3:2017 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAYS
    DIN EN 15309:2007-08 Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence
    BS EN 15309:2007 Characterization of waste and soil. Determination of elemental composition by X-ray fluorescence
    UNI EN 15410 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    10/30147493 DC : 0 BS EN 16174 - SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF AQUA REGIA SOLUBLE FRACTIONS OF ELEMENTS
    13/30272291 DC : 0 BS ISO 18227 - SOIL QUALITY - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    ISO 18227:2014 Soil quality Determination of elemental composition by X-ray fluorescence
    DIN EN 15410:2011-11 Solid recovered fuels - Method for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    UNE-EN 15410:2012 Solid recovered fuels - Methods for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    DIN EN 15309 E : 2007 CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    BS EN 15410:2011 (published 2011-09) Solid recovered fuels. Methods for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
    DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    BS ISO 18227 : 2014 SOIL QUALITY - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    BS EN 16457:2014 (published 2014-03) Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
    DIN EN 16174:2012-11 Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
    BS PD CLC/TS 50625-3-3 : 2017 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAYS
    CLC/TS 50625-3-3 : 2017 Collection, logistics & treatment requirements for WEEE - Part 3-3: Specification for de-pollution - WEEE containing CRTs and flat panel displays
    04/30116791 DC : DRAFT JUL 2004 BS EN 15002 - CHARACTERISATION OF WASTE - PREPARATION OF TEST PORTIONS FROM LABORATORY SAMPLE
    I.S. EN 15410:2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    UNI EN 16174 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF AQUA REGIA SOLUBLE FRACTIONS OF ELEMENTS
    DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. EN 16174:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF AQUA REGIA SOLUBLE FRACTIONS OF ELEMENTS
    CEI CLC/TS 50625-3-3 : 1ED 2018 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-3: SPECIFICATION FOR DE-POLLUTION - WEEE CONTAINING CRTS AND FLAT PANEL DISPLAY
    BS EN 16174:2012 (published 2012-09) Sludge, treated biowaste and soil. Digestion of aqua regia soluble fractions of elements
    I.S. EN 15309:2007 CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
    DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    17/30348303 DC : 0 BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
    UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    BS EN 15002:2015 (published 2015-04) Characterization of waste. Preparation of test portions from the laboratory sample
    13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 15410 : 2011 SOLID RECOVERED FUELS - METHODS FOR THE DETERMINATION OF THE CONTENT OF MAJOR ELEMENTS (AL, CA, FE, K, MG, NA, P, SI, TI)
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 15309:2007 Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence
    EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    EN 16174 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF AQUA REGIA SOLUBLE FRACTIONS OF ELEMENTS

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results Part 1: General principles and definitions
    ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
    EN 1483 : 2007 WATER QUALITY - DETERMINATION OF MERCURY - METHOD USING ATOMIC ABSORPTION SPECTROMETRY
    EN ISO 5961 : 1995 WATER QUALITY - DETERMINATION OF CADMIUM BY ATOMIC ABSORPTION SPECTROMETRY (ISO 5961:1994)
    ISO 5961:1994 Water quality Determination of cadmium by atomic absorption spectrometry
    ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results Part 3: Intermediate measures of the precision of a standard measurement method
    ENV 12506 : DRAFT 2000 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, CD, CR (6), CU, NI, PB, ZN, CL[-], NO[2][-], SO[4][2-]
    ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
    ISO 8288:1986 Water quality — Determination of cobalt, nickel, copper, zinc, cadmium and lead — Flame atomic absorption spectrometric methods
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
    EN 1233 : 1996 WATER QUALITY - DETERMINATION OF CHROMIUM - ATOMIC ABSORPTION SPECTROMETRIC METHODS
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    EN ISO 3696 : 1995 WATER FOR ANALYTICAL LABORATORY USE - SPECIFICATION AND TEST METHODS (ISO 3696:1987)
    EN ISO 11969:1996 WATER QUALITY - DETERMINATION OF ARSENIC - ATOMIC ABSORPTION SPECTROMETRIC METHOD (HYDRIDE TECHNIQUE)
    ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
    EN 45001 : 1989 GENERAL CRITERIA FOR THE OPERATION OF TESTING LABORATORIES
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