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EN 13925-2:2003

Current
Current

The latest, up-to-date edition.

Non-destructive testing - X-ray diffraction from polycrystalline and amorphous materials - Part 2: Procedures
Published date

12-03-2003

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Specimen preparation
  4.1 General preparation
  4.2 Block specimens
  4.3 Powder specimens
  4.4 Analysis of small quantities of sample
  4.5 Reactive samples and non-ambient conditions
5 Data collection
  5.1 General considerations
  5.2 Angular range and mode of data collection
  5.3 Parameters relevant to the quality of collected data
6 Data processing and analysis
  6.1 Background
  6.2 Peal searching
  6.3 Pattern decomposition into individual line profiles
      including background subtraction
  6.4 Phase identification
  6.5 Indexing
  6.6 Lattice parameter refinement
  6.7 Other types of analysis
Annex A (informative) Relationship between the XRPD standards
Annex B (informative) Example of Report Form
Annex C (informative) Scheme of a typical procedure for
        XRPD measurements
Annex D (informative) Some analytical functions used for
        profile fitting
Annex E (informative) Some methods for testing the internal
        consistency of XRPD data
        E.1 General
        E.2 Figures of Merit for FWHMs and intensities
        E.3 Figures of Merit for line positions and lattice
            parameters
Bibliography

This standard outlines the basic procedures applied in the X-ray Powder Diffraction (XRPD) method. Many of these procedures are common to most types of diffractometer used and type of analysis mentionen in prEN WI 00138079 (General Principles). In the interests of clarity and immediate usability more detail is given for procedures using instruments with Bragg-Brentano geometry and application to phase identification. Aspects of specimen preparation and data quality assessment are included, but the standard remains non-exhaustive.

Committee
CEN/TC 138
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

DD ISO/TS 12805:2011 Nanotechnologies. Materials specifications. Guidance on specifying nano-objects
BS EN 13925-3:2005 Non-destructive testing. X-ray diffraction from polycrystalline and amorphous materials Instruments
EN 1330-11:2007 Non-destructive testing - Terminology - Terms used in X-ray diffraction from polycrystalline and amorphous materials
DD CEN ISO/TS 21432:2005 Non-destructive testing. Standard test method for determining residual stresses by neutron diffraction
PD ISO/TS 11937:2012 Nanotechnologies. Nanoscale titanium dioxide in powder form. Characteristics and measurement
DIN EN 15049:2007-12 Railway applications - Suspension components - Torsion bar, steel
PREN 15305 : DRAFT 2005 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
04/19973037 DC : DRAFT OCT 2004 BS EN 1330-11 - NON-DESTRUCTIVE TESTING - TERMINOLOGY - PART 11: X-RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS
DIN EN 15305:2009-01 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
ISO/TS 11931:2012 Nanotechnologies — Nanoscale calcium carbonate in powder form — Characteristics and measurement
ISO/TS 12805:2011 Nanotechnologies Materials specifications Guidance on specifying nano-objects
I.S. CEN ISO TS 21432:2005 NON-DESTRUCTIVE TESTING - STANDARDS TEST METHOD FOR DETERMINING RESIDUAL STRESSES BY NEUTRON DIFFRACTION
UNI EN 13925-3 : 2005 NON-DESTRUCTIVE TESTING - X RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 3: INSTRUMENTS
DIN EN 15305 E : 2009 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
BS EN 15305:2008 Non-destructive testing. Test method for residual stress analysis by X-ray diffraction
05/30137047 DC : 0 EN 15305 - NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
UNI EN 15305 : 2008 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
I.S. EN 15305:2008 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
CEN ISO/TS 21432:2005/AC:2009 NON-DESTRUCTIVE TESTING - STANDARDS TEST METHOD FOR DETERMINING RESIDUAL STRESSES BY NEUTRON DIFFRACTION
ISO/TS 11937:2012 Nanotechnologies — Nanoscale titanium dioxide in powder form — Characteristics and measurement
DIN EN 15049 E : 2007 RAILWAY APPLICATIONS - SUSPENSION COMPONENTS - TORSION BAR, STEEL
BS EN 1330-11:2007 Non-destructive testing. Terminology Terms used in X-ray diffraction from polycrystalline and amorphous materials
BS EN 13925-1:2003 Non-destructive testing. X-ray diffraction from polycrystalline and amorphous materials General principles
BS EN 15049:2007 Railway applications. Suspension components. Torsion bar, steel
EN 13925-1:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous material - Part 1: General principles
EN 15049:2007 Railway applications - Suspension components - Torsion bar, steel
EN 13925-3:2005 Non destructive testing - X ray diffraction from polycrystalline and amorphous materials - Part 3: Instruments
PD ISO/TS 11931:2012 Nanotechnologies. Nanoscale calcium carbonate in powder form. Characteristics and measurement
ISO/TS 21432:2005 Non-destructive testing Standard test method for determining residual stresses by neutron diffraction
DIN EN 13925-1:2003-07 NON-DESTRUCTIVE TESTING - X-RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 1: GENERAL PRINCIPLES
DIN EN 13925-3:2005-07 NON-DESTRUCTIVE TESTING - X RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 3: INSTRUMENTS
EN 15305:2008/AC:2009 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
EN 13925-1:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous material - Part 1: General principles

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