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EN 13925-3:2005

Current

Current

The latest, up-to-date edition.

Non destructive testing - X ray diffraction from polycrystalline and amorphous materials - Part 3: Instruments

Published date

04-05-2005

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Description of equipment
   4.1 General
   4.2 X-ray sources
        4.2.1 General
        4.2.2 Conventional X-ray sources (sealed tubes and
               rotating anode sources)
        4.2.3 Synchrotron radiation sources
   4.3 Incident and diffracted X-ray beam optics
        4.3.1 General
        4.3.2 Monochromators
        4.3.3 Beam dimensions and geometry
   4.4 Detectors
        4.4.1 Types of detector
        4.4.2 Spatial resolution of detectors
        4.4.3 Energy resolution of detectors
   4.5 Goniometers
        4.5.1 General
        4.5.2 Specimen positioning
   4.6 Specimen stage
   4.7 Data collection system
5 Characterisation of equipment components
6 Equipment alignment and calibration
   6.1 General
   6.2 Alignment
   6.3 Calibration
7 Performance testing and monitoring
Annex A (informative) Relationship between the XRPD standards
Annex B (informative) Alignment of Bragg-Brentano diffractometers
Annex C (informative) Procedures for instrument performance
        characterisation
 C.1 General
 C.2 Position, intensity and breadth of a limited number of
      diffraction lines
 C.3 Angular Deviation Curve
 C.4 Line breadth
 C.5 Intensity diagrams
 C.6 Shape Analysis Curve
 C.7 Lattice parameters
 C.8 The use of the Fundamental Parameter Approach
 C.9 Whole pattern fitting
Annex D (informative) Sample report forms for characterisation of
        instruments
Bibliography

This document sets out the characteristics of instruments used for X-ray powder diffraction ("powder" as defined in EN 13925-1:2003, Clause 5) as a basis for their control and hence quality assurance of the measurements made by this technique. Performance testing indicators are given for diffractometer performance testing. Different types and makes of X-ray powder diffractometer vary considerably in their design and intended fields of application. This document attempts to cover as much of this range as possible by keeping to common principles. To make the standard more readily applicable, the Bragg-Brentano configuration is addressed in most detail because of its wide use. Additional considerations and adaptations may be necessary to cover some types of instruments or configuration and some fields of application. Some of these types of instrument are described in Annex B.

Committee
CEN/TC 138
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

DD ISO/TS 12805:2011 Nanotechnologies. Materials specifications. Guidance on specifying nano-objects
EN 1330-11:2007 Non-destructive testing - Terminology - Terms used in X-ray diffraction from polycrystalline and amorphous materials
DD CEN ISO/TS 21432:2005 Non-destructive testing. Standard test method for determining residual stresses by neutron diffraction
PD ISO/TS 11937:2012 Nanotechnologies. Nanoscale titanium dioxide in powder form. Characteristics and measurement
PREN 15305 : DRAFT 2005 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
DIN EN 15305:2009-01 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
ISO/TS 11931:2012 Nanotechnologies — Nanoscale calcium carbonate in powder form — Characteristics and measurement
ISO/TS 12805:2011 Nanotechnologies Materials specifications Guidance on specifying nano-objects
I.S. CEN ISO TS 21432:2005 NON-DESTRUCTIVE TESTING - STANDARDS TEST METHOD FOR DETERMINING RESIDUAL STRESSES BY NEUTRON DIFFRACTION
DIN EN 15305 E : 2009 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
BS EN 15305:2008 Non-destructive testing. Test method for residual stress analysis by X-ray diffraction
05/30137047 DC : 0 EN 15305 - NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
UNI EN 15305 : 2008 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
I.S. EN 15305:2008 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION
CEN ISO/TS 21432:2005/AC:2009 NON-DESTRUCTIVE TESTING - STANDARDS TEST METHOD FOR DETERMINING RESIDUAL STRESSES BY NEUTRON DIFFRACTION
ISO/TS 11937:2012 Nanotechnologies — Nanoscale titanium dioxide in powder form — Characteristics and measurement
BS EN 1330-11:2007 Non-destructive testing. Terminology Terms used in X-ray diffraction from polycrystalline and amorphous materials
PD ISO/TS 11931:2012 Nanotechnologies. Nanoscale calcium carbonate in powder form. Characteristics and measurement
ISO/TS 21432:2005 Non-destructive testing Standard test method for determining residual stresses by neutron diffraction
EN 15305:2008/AC:2009 NON-DESTRUCTIVE TESTING - TEST METHOD FOR RESIDUAL STRESS ANALYSIS BY X-RAY DIFFRACTION

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
EN 13925-1:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous material - Part 1: General principles
EN 13925-2:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous materials - Part 2: Procedures

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