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  • EN 14538:2006

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    Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

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    Published date:  07-06-2006

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Chemicals
    5 Apparatus
    6 Sampling
    7 Preparation of the calibration solutions and the
       blank solution
       7.1 General
       7.2 Blank solution
       7.3 Calibration solution with a nominal element
           content of 0,5 mg/kg
       7.4 Calibration solution with a nominal element
           content of 1 mg/kg
       7.5 Calibration solution with a nominal element
           content of 5 mg/kg
       7.6 Calibration solution with a nominal element
           content of 10 mg/kg
    8 Calibration
       8.1 General
       8.2 Calibration
       8.3 Check of calibration
    9 Sample analysis
       9.1 Sample preparation
       9.2 Measurement
    10 Calculation
    11 Results
    12 Precision
       12.1 Repeatability
       12.2 Reproducibility
    13 Test report

    Abstract - (Show below) - (Hide below)

    This document specifies a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 19
    Development Note Supersedes PREN 14538. (12/2007)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    15/30303049 DC : 0 BS ISO 21033 - ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
    BS ISO 21033:2016 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
    BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
    CEN/TR 17144 : 2017 RESISTANCE OF METALLIC MATERIALS TO LIQUID BIOGENIC AND ALTERNATIVE FUELS AND THEIR BLENDS
    BS PD ISO/TS 21033 : 2011 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
    DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    S.R. CEN/TR 17144:2017 RESISTANCE OF METALLIC MATERIALS TO LIQUID BIOGENIC AND ALTERNATIVE FUELS AND THEIR BLENDS
    DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    DD ISO/TS 21033 : 2011 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
    ISO 21033:2016 Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES)
    UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    ISO/TS 21033:2011 Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES)
    PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    PD CEN/TR 17144:2017 RESISTANCE OF METALLIC MATERIALS TO LIQUID BIOGENIC AND ALTERNATIVE FUELS AND THEIR BLENDS
    DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    ISO 3170:2004 Petroleum liquids Manual sampling
    EN ISO 3170 : 2004 PETROLEUM LIQUIDS - MANUAL SAMPLING (ISO 3170:2004)
    EN ISO 3171 : 1999 PETROLEUM LIQUIDS - AUTOMATIC PIPELINE SAMPLING
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