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EN 1528-3 : 1996

Current
Current

The latest, up-to-date edition.

FATTY FOOD - DETERMINATION OF PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCB'S) - PART 3: CLEAN-UP METHODS
Published date

20-11-1996

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 General
5 Method A: Liquid-liquid partitioning with acetonitrite
   and clean-up on a Florisil column (AOAC)
6 Method B: Liquid-liquid partitioning with
   dimethylformamide and clean-up on a Florisil (AOAC)
7 Method C: Column chromatography on activated
   Florisil (AOAC)
8 Method D: Column chromatography on partially deactivated
   Florisil (Stijve)
9 Method E: Column chromatography on partially
   deactivated aluminium oxide (Greve & Grevenstuk)
10 Method F: Gel permeation chromatography (GPC) (AOAC)
11 Method G: Gel permeation chromatography (GPC) and column
   chromatography on partially deactivated silica gel
   (Specht)
12 Method H: High performance gel permeation chromatography
   (HPGPC) (MAFF)
Annex A (informative) Purification of some solvents
Annex B (informative) Bibliography

This part of EN 1528 specifies the details of methods A to H for the clean-up of fats and oils or the isolated fat portion, respectively, using techniques such as liquid/liquid partition, adsorption or gel permeation column chromatography.

Committee
TC 275
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

EN 12918 : 1999 WATER QUALITY - DETERMINATION OF PARATHION, PARATHION-METHYL AND SOME OTHER ORGANOPHOSPHORUS COMPOUNDS IN WATER BY DICHLOROMETHANE EXTRACTION AND GAS CHROMATOGRAPHIC ANALYSIS
BS 6068-2.67(1999) : 1999 WATER QUALITY - DETERMINATION OF PARATHION, PARATHION-METHYL AND SOME OTHER ORGANOPHOSPHORUS COMPOUNDS IN WATER BY DICHLOROMETHANE EXTRACTION AND GAS CHROMATOGRAPHIC ANALYSIS
EN 1528-1:1996 Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 1: General
EN 1528-2 : 1996 FATTY FOOD - DETERMINATION OF PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBS) - PART 2: EXTRACTION OF FAT, PESTICIDES AND PCBS, AND DETERMINATION OF FAT CONTENT
EN 1528-4 : 1996 FATTY FOOD - DETERMINATION OF PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCB'S) - PART 4: DETERMINATION, CONFIRMATORY TESTS, MISCELLANEOUS
BS EN 12918:1999 Water quality. Determination of parathion, parathion-methyl and some other organophosphorus compounds in water by dichloromethane extraction and gas chromatographic analysis

EN 1528-4 : 1996 FATTY FOOD - DETERMINATION OF PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCB'S) - PART 4: DETERMINATION, CONFIRMATORY TESTS, MISCELLANEOUS
EN 1528-1:1996 Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 1: General
EN 1528-2 : 1996 FATTY FOOD - DETERMINATION OF PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBS) - PART 2: EXTRACTION OF FAT, PESTICIDES AND PCBS, AND DETERMINATION OF FAT CONTENT

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