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EN 16143:2013

Current
Current

The latest, up-to-date edition.

Petroleum products - Determination of content of Benzo(a)pyrene (BaP) and selected polycyclic aromatic hydrocarbons (PAH) in extender oils - Procedure using double LC cleaning and GC/MS analysis
Published date

13-02-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling and sample handling
8 Clean-up procedure
9 Test procedure
10 Expression of results
11 Precision
12 Test report
Annex A (normative) - Relevant physical chemical data
        for PAHs
Annex B (informative) - Additional user information
Bibliography

This European Standard specifies a procedure for the determination of the content of benzo[a]pyrene (BaP) in extender oils which are commonly used in the rubber industry for the production of tyres or parts of tyres. The method also yields the sum of the eight individual polycyclic aromatic hydrocarbons (PAHs) listed in Table 1. The procedure has been tested and verified for the PAHs listed in Table 1 (those required by the European Commission [1]) and additional PAHs as listed in Table A.2. Analysis of other PAHs is possible in principle, but sufficient quality assurance performed by the user is necessary to secure the analysis. The application range for this method is from approximately 4 mg/kg to approximately 15 mg/kg for the eight individual PAHs and from approximately 0,5 mg/kg to approximately 2 mg/kg for BaP.NOTE 1The intended working range for this method is in the 0,1 mg/kg to 15 mg/kg range. For the lower levels precision has not yet been established.NOTE 2For the purposes of this European Standard, the term "% (m/m)" is used to represent the mass fraction (...).(...)

Committee
CEN/TC 19
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
IP 605 : 2014 Identical
DIN EN 16143:2013-05 Identical
NF EN 16143 : 2013 Identical
PN EN 16143 : 2013 Identical
NS EN 16143 : 2013 Identical
BS EN 16143:2013 Identical
UNE-EN 16143:2013 Identical
UNI EN 16143 : 2013 Identical
I.S. EN 16143:2013 Identical
SN EN 16143 : 2013 Identical
NBN EN 16143 : 2013 Identical
BS 2000-605(2013) : 2013 Identical
NEN EN 16143 : 2013 Identical

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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