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CEN
EN 16319:2013+A1:2015

EN 16319:2013+A1:2015

Current

Current

The latest, up-to-date edition.

Fertilizers and liming materials - Determination of cadmium, chromium, lead and nickel by inductively coupled plasma-atomic emission spectrometry (ICP-AES) after aqua regia dissolution

Published date

23-12-2015

Publisher

Comite Europeen de Normalisation

European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Sampling and sample preparation
6 Reagents
7 Apparatus
8 Procedure
9 Calculation and expression of the results
10 Precision
11 Test report
Annex A (informative) - Results of the inter-laboratory test
Bibliography

This European Standard specifies a method for the determination of the content of cadmium, chromium, nickel and lead in fertilizers with inductively coupled plasma atomic emission spectrometry (ICP-AES) after extraction with aqua regia. Limits of quantification are dependent on the sample matrix as well as on the instrument, but can roughly be expected to be 0,3 mg/kg for Cd and 1 mg/kg for Cr, Ni and Pb.NOTEDue to significant interference from Cu, Fe and Mn, no valid results can be reported using this method for fertilizer matrices containing high concentrations (>/= 10 %) of these micro-nutrients.

Committee
CEN/TC 260
DevelopmentNote
Supersedes PREN 16319 & CEN/TS 16319. (10/2013) 2013 Edition Re-Issued in December 2015 & incorporates AMD 1 2015. (01/2016)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

I.S. EN 16964:2018 FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS USING AQUA REGIA
EN 16964:2018 Fertilizers - Extraction of total micro-nutrients in fertilizers using aqua regia
EN 16963:2018 Fertilizers - Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES
14/30250835 DC : 0 BS ISO 17318 - FERTILIZERS AND SOIL CONDITIONERS - DETERMINATION OF ARSENIC, CADMIUM, CHROMIUM, LEAD AND MERCURY CONTENTS
16/30330776 DC : 0 BS EN 16963 - FERTILIZERS - DETERMINATION OF BORON, COBALT, COPPER, IRON, MANGANESE, MOLYBDENUM AND ZINC USING ICP-AES
16/30330779 DC : 0 BS EN 16964 - FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS AND REMOVAL OF ORGANIC COMPOUNDS FROM FERTILIZER EXTRACTS
I.S. EN 16963:2018 FERTILIZERS - DETERMINATION OF BORON, COBALT, COPPER, IRON, MANGANESE, MOLYBDENUM AND ZINC USING ICP-AES

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
EN 12944-2:1999/AC:2000 FERTILIZERS AND LIMING MATERIALS AND SOIL IMPROVERS - VOCABULARY - PART 2: TERMS RELATING TO FERTILIZERS
EN 12944-1:1999/AC:2000 FERTILIZERS AND LIMING MATERIALS AND SOIL IMPROVERS - VOCABULARY - PART 1: GENERAL TERMS
EN 1482-2:2007 Fertilizers and liming materials - Sampling and sample preparation - Part 2: Sample preparation
EN 12944-3 : 2001 FERTILIZERS AND LIMING MATERIALS - VOCABULARY - PART 3: TERMS RELATING TO LIMING MATERIALS
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 1482-1:2007 Fertilizers and liming materials - Sampling and sample preparation - Part 1: Sampling

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