Name: EN 16691:2015
Brand: CEN

WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)

Published date

23-09-2015

Publisher

Comite Europeen de Normalisation

European foreword
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Measurement of samples
11 Identification of individual compounds by means
   of GC-MS (SIM)
12 Calculation
13 Expression of results
14 Test report
Annex A (informative) - Suitable gas chromatographic
        conditions and example chromatograms -
        GC-conditions
Annex B (informative) - Repeatability and reproducibility data
Annex C (informative) - Dilution Schedules for standards
Annex D (informative) - Silica clean-up
Annex E (informative) - Examples of suitable solid-phase
        extraction disks (SPE-disks)
Bibliography

This European Standard specifies a method for the determination of 7 polycyclic aromatic hydrocarbons (PAH) in whole water samples as listed in Table 1.

Committee	CEN/TC 230
DevelopmentNote	Supersedes PREN 16691. (09/2015)
DocumentType	Standard
PublisherName	Comite Europeen de Normalisation
Status	Current

Standards	Relationship
SN EN 16691 : 2015	Identical
BS EN 16691:2015	Identical
NEN EN 16691 : 2015	Identical
NF EN 16691 : 2015	Identical
UNE-EN 16691:2016	Identical
UNI EN 16691 : 2015	Identical
NBN EN 16691 : 2015	Identical
DIN EN 16691 E : 2015	Identical
DIN EN 16691:2015-12	Identical
I.S. EN 16691:2015	Identical
NS EN 16691 : 2015	Identical
PN EN 16691 : 2015	Identical

ISO 7981-1:2005	Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 1: Determination of six PAH by high-performance thin-layer chromatography with fluorescence detection after liquid-liquid extraction
EN ISO 17993 : 2003	WATER QUALITY - DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WATER BY HPLC WITH FLUORESCENCE DETECTION AFTER LIQUID-LIQUID EXTRACTION
NEN 7777 : 2011 + C1 2012	ENVIRONMENT AND FOOD - PERFORMANCE CHARACTERISTICS OF MEASUREMENT METHODS
ISO 1042:1998	Laboratory glassware One-mark volumetric flasks
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 7981-2:2005	Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 2: Determination of six PAH by high-performance liquid chromatography with fluorescence detection after liquid-liquid extraction
ISO 17993:2002	Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
EN ISO 1042 : 1999	LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 28540:2011	Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
ISO 6107-2:2006	Water quality Vocabulary Part 2:
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN 15527:2008	Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
ISO/TS 28581:2012	Water quality — Determination of selected non-polar substances — Method using gas chromatography with mass spectrometric detection (GC-MS)
EN ISO 5667-1 : 2006 COR 2007	WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES