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  • IEC 61619:1997

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    Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography

    Available format(s):  Hardcopy, PDF, PDF 3 Users, PDF 5 Users, PDF 9 Users

    Language(s):  English - French, Spanish, Castilian

    Published date:  10-04-1997

    Publisher:  International Electrotechnical Committee

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    Table of Contents - (Show below) - (Hide below)

    CONTENTS
    FOREWORD
    Clause
    1. Scope
    2. Normative reference
    3. Definitions
    4. Principle
    5. Reagents and auxilliary materials
    6. Apparatus
    7. Sample
    8. Chromatograph operating conditions
    9. Data-processing system
    10. Checks of instrumental performance
    11. Procedure
    12. Test report
    13. Detection limit
    14. Precision
    Annexes
    A Test mixtures
    B General informations
    C Bibliography

    Abstract - (Show below) - (Hide below)

    Specifies a method for the determination of polychlorinated biphenyl (PCB) concentration in non-halogenated insulating liquids by high-resolution capillary column gas chromatography using an electron capture detector (ECD). Gives total PCB content; especially useful when a detailed analysis of PCB congeners is necessary.

    General Product Information - (Show below) - (Hide below)

    Development Note Supersedes IEC 60997 (05/2002) Also numbered as BS EN 61619. (09/2005) Stability Date: 2019. (10/2012)
    Document Type Standard
    Publisher International Electrotechnical Committee
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    11/30235371 DC : 0 BS EN 62701 - FLUIDS FOR ELECTRO TECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
    BS EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 60422:2013 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
    BS 2000-462.3(2004) : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    UNE-EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
    17/30331680 DC : 0 BS ISO 18095 - CONDITION MONITORING AND DIAGNOSTICS OF POWER TRANSFORMERS
    12/30257150 DC : 0 BS EN 62770 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS LIQUIDS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
    BS EN 62770:2014 Fluids for electrotechnical applications. Unused natural esters for transformers and similar electrical equipment
    06/30159746 DC : 0 BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    BS EN 60422:2013 (published 2014-03) Mineral insulating oils in electrical equipment. Supervision and maintenance guidance
    02/207269 DC : 0 IEC 60422 ED.3 - SUPERVISION AND MAINTENANCE GUIDE FOR MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT
    BS EN 60296 : 2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
    03/100561 DC : DRAFT JULY 2003 IEC 60422 ED.3 - SUPERVISION AND MAINTENANCE GUIDE FOR MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT
    15/30330799 DC : 0 BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    00/244591 DC : DRAFT OCT 2000 SPECIFICATION FOR UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
    10/30215366 DC : 0 BS EN 60422 - MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
    CLC/TR 50503 : 2010 Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs
    S.R. CLC/TR 50503:2010 GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    PREN 15308 : DRAFT 2015 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
    I.S. EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
    I.S. EN 62770:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
    DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 62701:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
    IEC 60296 REDLINE : 4.0 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
    BS 2000-462.2(2001) : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    09/30213528 DC : 0 BS EN 60296 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OIL FOR TRANSFORMERS AND SWITCHGEAR
    ISO 18095:2018 Condition monitoring and diagnostics of power transformers
    CEI EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
    ISO 13876:2013 Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    I.S. EN 12766-2:2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    I.S. EN 12766-3:2005 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    CEI EN 60296 : 2013 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
    DIN EN 12766-3:2005-02 Petroleum products and used oils - Determination of PCBs and related products - Part 3: Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
    IEC 62770:2013 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
    BS EN 12766-3 : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    BS EN 12766-2 : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    IEC 60296:2012 RLV Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
    UNE-EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
    UNE-EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
    IEC 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
    EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012)
    EN 62701 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS (IEC 62701:2014)
    EN 12766-2 : 2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    EN 12766-3:2004/AC:2007 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT (IEC 62770:2013)
    EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
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