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IEC 62535:2008

Current
Current

The latest, up-to-date edition.

Insulating liquids - Test method for detection of potentially corrosive sulphur in used and unused insulating oil
Available format(s)

Hardcopy , PDF , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

English - French, Spanish, Castilian

Published date

08-10-2008

IEC 62535:2008 specifies a test method for detection of potentially corrosive sulphur in used and unused mineral insulating oil. Most recent failures due to corrosive sulphur are related to the formation of copper sulphide deposits in and on the surface of winding cellulosic paper. The test method uses a copper conductor, wrapped with one layer of paper, immersed in the oil and heated to evaluate the capability of the oil to yield copper sulphide and transfer it to paper layers. The growth of copper sulphide on bare copper may cause the presence of conductive particulates in the oil, which can act as nuclei for electrical discharge and may lead to a fault. Other test methods exist using a bare copper strip immersed in oil and heated to detect the corrosive behaviour of oil against copper. ASTM D1275 Method B is also used for this test and a modified procedure using low oil volumes is included in Annex A. Tests with and without paper are considered as complementary and may lead to different results.

Committee
TC 10
DevelopmentNote
Stability Date: 2022. (12/2017)
DocumentType
Standard
Pages
32
PublisherName
International Electrotechnical Committee
Status
Current

Standards Relationship
NF EN 62535 : 2009 Identical
NEN EN IEC 62535 : 2009 Identical
I.S. EN 62535:2009 Identical
PN EN 62535 : 2009 Identical
DIN EN 62535 : 2009 Identical
VDE 0370-33 : 2009 Identical
BS EN 62535:2009 Identical
CEI EN 62535 : 2009 Identical
EN 62535:2009 Identical
UNE-EN 62535:2009 Identical

09/30213528 DC : 0 BS EN 60296 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OIL FOR TRANSFORMERS AND SWITCHGEAR
BS EN 60422:2013 Mineral insulating oils in electrical equipment. Supervision and maintenance guidance
12/30257150 DC : 0 BS EN 62770 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS LIQUIDS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
S.R. CLC/TR 50503:2010 GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
PD IEC/TR 62697-3:2018 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids Test method for quantitative determination of elemental sulfur
CEI EN 62040-4 : 2014 UNINTERRUPTIBLE POWER SYSTEMS (UPS) - PART 4: ENVIRONMENTAL ASPECTS - REQUIREMENTS AND REPORTING
I.S. EN 62701:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
I.S. EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
IEC TR 62697-2:2018 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 2: Test method for quantitative determination of total corrosive sulfur (TCS)
I.S. EN 62697-1:2012 TEST METHODS FOR QUANTITATIVE DETERMINATION OF CORROSIVE SULFUR COMPOUNDS IN UNUSED AND USED INSULATING LIQUIDS - PART 1: TEST METHOD FOR QUANTITATIVE DETERMINATION OF DIBENZYLDISULFIDE (DBDS) (IEC 62697-1:2012 (EQV))
IEC 60296 REDLINE : 4.0 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
EN 62040-4:2013 Uninterruptible power systems (UPS) - Part 4: Environmental aspects - Requirements and reporting
EN 62697-1:2012 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 1: Test method for quantitative determination of dibenzyldisulfide (DBDS)
EN 62701:2014 Fluids for electrotechnical applications - Recycled mineral insulating oils for transformers and switchgears
OVE EN IEC 60296:2023 01 01 Fluids for electrotechnical applications - Mineral insulating oils for electrical equipment
I.S. EN 60422:2013 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
10/30233636 DC : 0 IEC 62697-1 ED.1 - INSULATING LIQUIDS - QUANTITATIVE DETERMINATION OF CORROSIVE SULFUR COMPOUNDS IN USED AND UNUSED INSULATING LIQUIDS - PART 1: TEST METHOD FOR QUANTITATIVE DETERMINATION OF DIBENZYL DISULFIDE (DBDS)
BS EN 62697-1:2012 Test methods for quantitative determination of corrosive sulphur compounds in unused and used insulating liquids Test method for quantitative determination of dibenzyldisulfide (DBDS)
17/30331680 DC : 0 BS ISO 18095 - CONDITION MONITORING AND DIAGNOSTICS OF POWER TRANSFORMERS
BS EN 60296:2012 Fluids for electrotechnical applications. Unused mineral insulating oils for transformers and switchgear
10/30215366 DC : 0 BS EN 60422 - MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
NF EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
I.S. EN 62040-4:2013 UNINTERRUPTIBLE POWER SYSTEMS (UPS) - PART 4: ENVIRONMENTAL ASPECTS - REQUIREMENTS AND REPORTING (IEC 62040-4:2013 (EQV))
CEI EN 60296 : 2013 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
IEC 62770:2013 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
UNE-EN 62697-1:2013 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 1: Test method for quantitative determination of dibenzyldisulfide (DBDS)
EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
CEI EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
11/30235371 DC : 0 BS EN 62701 - FLUIDS FOR ELECTRO TECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
NF EN 62697-1 : 2013 LIQUIDES ISOLANTS - METHODES D'ESSAI POUR LA DETERMINATION QUANTITATIVE DES COMPOSES DE SOUFRE CORROSIF DANS LES LIQUIDES ISOLANTS USAGES ET NEUFS - PARTIE 1: METHODE D'ESSAI POUR LA DETERMINATION QUANTITATIVE DU DISULFURE DE DIBENZYLE (DBDS)
BS EN 62770:2014 Fluids for electrotechnical applications. Unused natural esters for transformers and similar electrical equipment
BS EN 62040-4:2013 Uninterruptible power systems (UPS) Environmental aspects. Requirements and reporting
IEEE C57.140-2006 IEEE Guide for Evaluation and reconditioning of Liquid Immersed Power Transformers
I.S. EN 62770:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
ISO 18095:2018 Condition monitoring and diagnostics of power transformers
I.S. EN 60079-6:2015 EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
IEC 60079-6:2015 Explosive atmospheres - Part 6: Equipment protection by liquid immersion "o"
UNE-EN 60079-6:2016 Explosive atmospheres - Part 6: Equipment protection by liquid immersion "o"
IEC 62040-4:2013 Uninterruptible power systems (UPS) - Part 4: Environmental aspects - Requirements and reporting
IEC 62697-1:2012 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 1: Test method for quantitative determination of dibenzyldisulfide (DBDS)
UNE-EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
UNE-EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
IEC 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
CAN/CSA-C50-14 (R2018) Mineral insulating oil, electrical, for transformers and switches
UNE-EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
13/30267448 DC : 0 BS EN 60079-6 ED 4.0 - EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
CEI EN 60079-6 : 2016 EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
BS EN 60079-6:2007 Explosive atmospheres Equipment protected by oil immersion \'o\'
CLC/TR 50503 : 2010 Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs
IEC TR 62697-3:2018 Test methods for quantitative determination of corrosive sulfur compounds in unused and used insulating liquids - Part 3: Test method for quantitative determination of elemental sulfur
IEC 60296:2012 RLV Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
EN 60079-6:2015 Explosive atmospheres - Part 6: Equipment protection by liquid immersion "o"
EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance

EN 13601:2013 Copper and copper alloys - Copper rod, bar and wire for general electrical purposes
IEC 60475:2011 Method of sampling insulating liquids
IEC 60567:2011 Oil-filled electrical equipment - Sampling of gases and analysis of free and dissolved gases - Guidance
ASTM D 1275 : 2015 Standard Test Method for Corrosive Sulfur in Electrical Insulating Liquids
IEC 60554-3-1:1979 Specification for cellulosic papers for electrical purposes. Part 3-1: Specifications for individual materials. General purpose electrical paper

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