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ISO 18857-2:2009

Current
Current

The latest, up-to-date edition.

Water quality Determination of selected alkylphenols Part 2: Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation
Available format(s)

Hardcopy , PDF , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

English, French

Published date

08-09-2009

ISO 18857-2:2009 specifies a gas chromatographic-mass spectrometric (GCMS) determination of selected alkylphenols, their ethoxylates and bisphenol A in non-filtered samples of drinking, ground, surface, and waste waters following solidphase extraction and derivatisation.

The lower limit of the working range depends on the matrix, on the specific compound to be analysed and on the sensitivity of the mass spectrometric detection unit. The method is applicable in a working range from 0,005 g/l to 0,2 g/l for 4-(1,1,3,3-tetramethylbutyl)phenol (OP), and its mono- (OP1EO) and diethoxylate (OP2EO), from 0,03 g/l to 0,2 g/l for 4-nonylphenol (mixture of isomers) (NP), and its mono- (NP1EO) and diethoxylate (NP2EO), and from 0,05 g/l to 0,2 g/l for bisphenol A (BPA).

Depending on the matrix, the method is also applicable to waste water in a working range from 0,1 g/l to 50 g/l for OP, OP1EO, OP2EO and BPA, and from 0,5 g/l to 50 g/l for NP, NP1EO and NP2EO. The working ranges are based on experimental work carried out in ruggedness testing. Water samples containing suspended matter at concentrations of more than 500 mg/l and waste water samples are extracted by passing a 100 ml sample through the cartridge.

DevelopmentNote
Supersedes ISO/DIS 18857-2. (09/2009)
DocumentType
Standard
Pages
18
PublisherName
International Organization for Standardization
Status
Current

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CEN/TS 16182:2012 Sludge treated biowaste and soil - Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates using gas chromatography with mass selective detection (GC-MS)

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ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006 Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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