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  • PREN 15308 : DRAFT 2015

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION

    Available format(s): 

    Superseded date:  01-10-2016

    Language(s): 

    Published date:  09-03-2016

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
    6 Apparatus
    7 Safety precautions
    8 Interferences
    9 Sample storage
    10 Pretreatment
    11 Procedure
    12 Calculation
    13 Test report
    Annex A (informative) - Performance characteristics
    Annex B (informative) - Examples of GC-MS chromatograms
            of a calibration standard solution and a contaminated
            soil sample
    Annex C (informative) - Examples of GC-ECD chromatograms
            of a calibration standard solution and a cable
            shredder sample
    Annex D (normative) - Calculation method for the estimation
            of total PCB content
    Annex E (informative) - Summary of general requirements and
            Recommendations
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection.

    General Product Information - (Show below) - (Hide below)

    Comment Closes On
    Committee TC 292
    Document Type Draft
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By

    Standards Referencing This Book - (Show below) - (Hide below)

    EN ISO 6468 : 1996 WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION
    EN 12766-1:2000 Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    EN 61619 : 1997 INSULATING LIQUIDS - CONTAMINATION BY POLYCHLORINATED BIPHENYLS (PCBS) - METHOD OF DETERMINATION BY CAPILLARY COLUMN GAS CHROMATOGRAPHY
    EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
    ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
    EN 12766-2 : 2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    IEC 61619:1997 Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
    ISO 6468:1996 Water quality Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes Gas chromatographic method after liquid-liquid extraction
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