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PREN 15308 : DRAFT 2015

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
Superseded date

01-10-2016

Published date

09-03-2016

European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Safety precautions
8 Interferences
9 Sample storage
10 Pretreatment
11 Procedure
12 Calculation
13 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Examples of GC-MS chromatograms
        of a calibration standard solution and a contaminated
        soil sample
Annex C (informative) - Examples of GC-ECD chromatograms
        of a calibration standard solution and a cable
        shredder sample
Annex D (normative) - Calculation method for the estimation
        of total PCB content
Annex E (informative) - Summary of general requirements and
        Recommendations
Bibliography

Defines a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection.

Committee
TC 292
DocumentType
Draft
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

Standards Relationship
15/30330799 DC : 0 Identical
05/30136951 DC : 0 Identical

EN ISO 6468 : 1996 WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION
EN 12766-1:2000 Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
EN 61619:1997 Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
IEC 61619:1997 Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
ISO 6468:1996 Water quality Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes Gas chromatographic method after liquid-liquid extraction

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