Name: PREN 17212 : DRAFT 2017
Brand: CEN

ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALSYSIS - DETERMINATION OF MELAMINE AND CYANURIC ACID CONTENT BYLIQUID CHROMATOGRAPHIC METHOD WITH MASS SPECTROMETRIC DETECTION (LC-MS/MS)

Published date

09-01-2018

Publisher

Comite Europeen de Normalisation

European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Preparation of sample
8 Procedure
9 HPLC-MS/MS analysis
10 Calculation
11 Precision
12 Test report
Annex A (informative) - Examples for suitable MS detection
        conditions
Annex B (informative) - Results of the international
        collaborative trial
Annex C (informative) - Results of the in-house validation
        of the method
Annex D (informative) - Typical chromatograms
Bibliography

Provides a high-performance liquid chromatographic (HPLC) mass spectrometric (MS) method for screening and quantification of melamine in the concentration range between < 1 mg/kg and 100 mg/kg feed.

Committee	TC 327
DocumentType	Draft
PublisherName	Comite Europeen de Normalisation
Status	Current

Standards	Relationship
NEN EN 17212 : DRAFT 2018	Identical
DIN EN 17212:2018-01 (Draft)	Identical
17/30337117 DC : DRAFT DEC 2017	Identical

ISO 5725-1:1994	Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 11843-2:2000	Capability of detection — Part 2: Methodology in the linear calibration case
ISO 24276:2006	Foodstuffs Methods of analysis for the detection of genetically modified organisms and derived products General requirements and definitions
EN ISO/IEC 17043:2010	Conformity assessment - General requirements for proficiency testing (ISO/IEC 17043:2010)
ISO 6497:2002	Animal feeding stuffs Sampling
ISO/IEC Guide 99:2007	International vocabulary of metrology Basic and general concepts and associated terms (VIM)
ISO 3534-2:2006	Statistics Vocabulary and symbols Part 2: Applied statistics
ISO/IEC 17043:2010	Conformity assessment — General requirements for proficiency testing
EN ISO 6498:2012	Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 6497 : 2005	ANIMAL FEEDING STUFFS - SAMPLING
ISO 6498:2012	Animal feeding stuffs — Guidelines for sample preparation
ISO 16577:2016	Molecular biomarker analysis — Terms and definitions