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UNI CEN/TS 16190 : 2012

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)

Superseded date

09-05-2022

Published date

01-01-2012

Foreword
Introduction
1 Scope
2 Normative references
3 Abbreviations
4 Principle
5 Reagents
6 Apparatus and materials
7 Sample storage and sample pretreatment
8 Extraction and clean-up
9 HRGC/HRMS analysis
10 Precision
11 Test report
Annex A (informative) - Toxic equivalent factors
Annex B (informative) - Repeatability and reproducibility
        data
Annex C (informative) - Examples of extraction and
        clean-up methods
Annex D (informative) - Examples of operation of GC/HRMS
        determination
Bibliography

Describes a method for quantitative determination of 17 2,3,7,8-chlorine substituted dibenzo-p-dioxins and dibenzofurans and dioxin-like polychlorinated biphenyls in sludge, treated biowaste and soil using liquid column chromatographic clean-up methods and GC/HRMS.

DocumentType
Standard
PublisherName
Ente Nazionale Italiano di Unificazione (UNI)
Status
Superseded
SupersededBy

Standards Relationship
CEN/TS 16190:2012 Identical

EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
EN 1948-1:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
ISO 18073:2004 Water quality — Determination of tetra- to octa-chlorinated dioxins and furans — Method using isotope dilution HRGC/HRMS
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment

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