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BS EN 62321-8 - DETERMINATION OF CERTAIN SUBSTANCES IN ELECTROTECHNICAL PRODUCTS - PART 8: PHTHALATES IN POLYMERS BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC- MS), PYROLYSIS/THERMAL DESORPTION-GAS CHROMATOGRAPHY-MASS SPECTROMETRY (PY/TD-GC-MS)

Available format(s)

Hardcopy , PDF

Superseded date

07-31-2017

Language(s)

English

Publisher

British Standards Institution

1. Scope
2. Normative references
3. Terms, definitions and abbreviations
4. Principle
5. Reagents and materials
6. Apparatus
7. Sampling
8. Procedure
9. Calculation of phthalate concentration
10. Precision
11. Quality assurance and control
12. Test report
Bibliography
Annex A (Informative) - Determination of Phthalates
        in polymers by Ion Attachment Mass Spectrometry
        (IAMS)
Annex B (Informative) - Determination of Phthalates in
        polymers by Liquid Chromatography-Mass
        Spectrometry(LC-MS)
Annex C (Informative) - Examples of chromatograms at
        suggested conditions
Annex D (Informative) - Verification of the EGA thermal
        desorption zone
Annex E (Informative) - Example of IAMS and Py/TD-GC-MS
        instruments
Annex F (Informative) - Example of false positive detection
        of phthalates
Annex G (Informative) - Examples of sample preparation for
        quantitative analysis of phthalates by GC-MS
Annex H (Informative) - Extraction of phthalates by dissolution
        in THF using sonication and precipitation of polymer matrix
Annex I (Informative) - Commercially available reference
        materials considered suitable for this analysis
Annex J (Informative) - Commercially available capillary
        columns considered suitable for this analysis
Annex K (Informative) - Labware cleaning procedure for
        phthalate testing
Annex L (Informative) - Results of international inter-laboratory
        study 5
Annex M (Informative) - Sample analysis sequence
Annex N (Informative) - Flow chart

BS EN 62321-8.

Committee	GEL/111
DocumentType	Draft
Pages	71
PublisherName	British Standards Institution
Status	Superseded
SupersededBy	BS EN 62321-8:2017

ISO/IEC 17025:2005	General requirements for the competence of testing and calibration laboratories
ISO/IEC Guide 98:1993	Guide to the expression of uncertainty in measurement (GUM)
ASTM D 7083 : 2016 : REDLINE	Standard Practice for Determination of Monomeric Plasticizers in Poly (Vinyl Chloride) (PVC) by Gas Chromatography
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
EN 14372:2004	Child use and care articles - Cutlery and feeding utensils - Safety requirements and tests