ASTM D 1552 : 2016 : EDT 1
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
Available format(s)
Hardcopy , PDF
Superseded date
05-31-2023
Language(s)
English
Published date
02-07-2017
1.1This test method covers procedures for the determination of total sulfur in petroleum products including lubricating oils containing additives, and in additive concentrates. This test method is applicable to samples boiling above 177 °C (350 °F) and containing a mass fraction of sulfur between 0.22 % and 24.2 %. Other sulfur concentrations may be analyzed, but the precision stated may or may not apply. These procedures use IR detection or TCD following combustion in a furnace.
1.2Petroleum coke containing a mass fraction of sulfur between 2.53 % to 3.79 % sulfur may be analyzed. Other sulfur concentrations may be analyzed, but the precision stated may or may not apply.
Note 1:The D1552–08 (2014) version of this standard contained two other procedures using iodate titrations. Since these procedures are no longer being used in the industry laboratories based on a survey of D02.SC 3 laboratories conducted in September 2014, they are being deleted. For earlier information on the deleted procedures, D1552–08 (2014) may be perused.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
6
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
| ASTM E 1219 : 2016 | Standard Practice for Fluorescent Liquid Penetrant Testing Using the Solvent-Removable Process |
| ASTM E 1210 : 2016 | Standard Practice for Fluorescent Liquid Penetrant Testing Using the Hydrophilic Post-Emulsification Process |
| ASTM D 6376 : 2010 : R2017 : EDT 1 | Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-ray Fluorescence Spectroscopy |
| ASTM E 1418 : 2016 | Standard Practice for Visible Penetrant Testing Using the Water-Washable Process |
| ASTM D 6443 : 2014 : R2019 : EDT 1 | Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure) |
| ASTM D 6448 : 2016 | Standard Specification for Industrial Burner Fuels from Used Lubricating Oils |
| ASTM D 3238 : 2017 : REV A | Standard Test Method for Calculation of Carbon Distribution and Structural Group Analysis of Petroleum Oils by the n-d-M Method |
| ASTM E 1220 : 2016 | Standard Practice for Visible Penetrant Testing Using Solvent-Removable Process |
| ASTM D 396 : 2019 | Standard Specification for Fuel Oils |
| ASTM E 165/E165M : 2018 | Standard Practice for Liquid Penetrant Testing for General Industry |
| ASTM D 240 : 2017 | Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter |
| ASTM D 8056 : 2018 | Standard Guide for Elemental Analysis of Crude Oil |
| ASTM D 7666 : 2012 | Standard Specification for Triglyceride Burner Fuel |
| ASTM D 6969 : 2017 | Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis |
| ASTM E 1208 : 2016 | Standard Practice for Fluorescent Liquid Penetrant Testing Using the Lipophilic Post-Emulsification Process |
| ASTM D 1266 : 2018 | Standard Test Method for Sulfur in Petroleum Products (Lamp Method) |
| ASTM D 7467 : 2019 | Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20) |
| ASTM D 6823 : 2008 : R2013 | Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils |
| ASTM D 4951 : 2014 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 3338/D3338M : 2009 : R2014 : EDT 2 | Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels |
| ASTM D 7455 : 2019 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
| ASTM D 4868 : 2017 | Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels |
| ASTM D 7578 : 2018 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM E 1209 : 2018 | Standard Practice for Fluorescent Liquid Penetrant Testing Using the Water-Washable Process |
| ASTM D 396 : 2021 | Standard Specification for Fuel Oils |
| ASTM D 7467 : 2020 : REV A | Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20) |
| ASTM D 240 : 2019 | Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter |
| ASTM D 7666 : 2012 : R2019 | Standard Specification for Triglyceride Burner Fuel |
| ASTM D 129 : 2018 | Standard Test Method for Sulfur in Petroleum Products (General High Pressure Decomposition Device Method) (Withdrawn 2023) |
| ASTM D 3338/D3338M : 2020 : REV A | Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels |
| ASTM D 975 : 2020 : REV C | Standard Specification for Diesel Fuel |
| ASTM D 7691 : 2016 | Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 5185 : 2018 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 2880 : 2020 | Standard Specification for Gas Turbine Fuel Oils |
| ASTM D 7578 : 2020 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 4951 : 2014 : R2019 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 4057 : 2019 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6300 : 2020 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6300 : 2013 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 4057 : 1995 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2010 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2014 : REV A : EDT 1 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6299 : 2013 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 2016 : EDT 1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2017 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2017 : REV B | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2017 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6299 : 2009 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 1995 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6300 : 2017 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 4057 : 2012 : R2018 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2013 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6792 : 2006 | Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6299 : 2021 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6792 : 2004 | Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6299 : 2010 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2016 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 4057 : 1981 : EDT 2 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6300 : 2004 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 2019 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6792 : 2004 : REV A | Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6300 : 2021 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6300 : 2019 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6792 : 2005 | Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6300 : 2020 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6299 : 2000 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2010 : EDT 2 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2016 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4057 : 2006 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 4177 : 2015 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2019 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2020 : REV B | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4057 : 2012 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2000 : REV A | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2006 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6792 : 2013 | Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6792 : 2017 | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
| ASTM D 6300 : 2014 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 2015 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 1999 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6792 : 2007 | Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6299 : 2020 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 1995 : R2010 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2008 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 1995 : R2000 | Standard Practice for Automatic Sampling of Peroleum and Petroleum Products |
| ASTM D 6300 : 2013 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6299 : 2002 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6300 : 2008 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 2003 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 2007 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6300 : 2002 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 4177 : 2016 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6792 : 2003 | Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 4177 : 1995 : R2005 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6300 : 2016 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 6792 : 2002 | Standard Guide for A Quality System in Petroleum Products and Lubricants Testing Laboratories |
| ASTM D 6299 : 2007 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2007 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4057 : 1995 : R2000 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2020 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2017 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 2015 : REV A | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6300 : 2014 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 4057 : 2006 : R2011 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2002 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
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