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ASTM D 2225 : 2004 : R2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods for Silicone Fluids Used for Electrical Insulation
Available format(s)

Hardcopy , PDF

Superseded date

11-12-2020

Language(s)

English

Published date

02-28-2013

CONTAINED IN VOL. 10.03, 2015 Defines the testing of silicone fluids for use in transformers, capacitors, and electronic assemblies as an insulating or cooling medium, or both.

1.1These test methods cover the testing of silicone fluids for use in transformers, capacitors, and electronic assemblies as an insulating or cooling medium, or both. These methods are generally suitable for specification acceptance, factory control, referee testing, and research.

1.2Although some of the test methods listed here apply primarily to petroleum-based fluids, they are, with minor revisions, equally applicable to silicone fluids.

1.3Silicone fluids are used for electrical insulating purposes because of their stable properties at high and low temperatures and their relative environmental inertness.

1.4A list of the properties and standards are as follows:

Property Measured

Section

ASTM Test Method

Physical:

 Color

6

D2129

 Flash point

7

D92

 Fire point

7

D92

 Polychlorinated biphenyl
  content

8

D4059

 Pour point

9

D97

 Refractive index

10

D1807

 Specific gravity

11

D1298, D1481, D4052

 Volatility

12

D4559

 Viscosity

13

D445, D2161

Chemical:

 Neutralization number

14

D974

 Water content

15

D1533

Electrical:

 Relative permittivity

16

D9242

 Dielectric breakdown
  voltage

17

D8773

 Dissipation factor

18

D9242

 Specific resistance

19

D11692

 Compatibility

20

D5282


1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 27
DocumentType
Test Method
Pages
4
ProductNote
Reconfirmed 2012
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 4652 : 2005 : R2012 Standard Specification for Silicone Fluid Used for Electrical Insulation
ASTM D 5282 : 2005 : R2012 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 877/D877M : 2013 Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using Disk Electrodes
ASTM D 1816 : 2012 Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using VDE Electrodes

ASTM D 2161 : 2005 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 2864 : 2009 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 2161 : 2019 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 1298 : 2012 : REV A Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 2161 : 2010 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 2161 : 1982 Standard Method for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 4052 : 1996 : R2002 : EDT 1 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D 1481 : 2017 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer (Withdrawn 2023)
ASTM D 1481 : 1991 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 1298 : 2012 : REV B Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 4652 : 2005 Standard Specification for Silicone Fluid Used for Electrical Insulation
ASTM D 1533 : 2012 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
ASTM D 2161 : 2010 : EDT 1 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1816 : 2012 : REDLINE Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using VDE Electrodes
ASTM D 4559 : 1999 : R2004 Standard Test Method for Volatile Matter in Silicone Fluid
ASTM D 1481 : 1993 : R1997 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 4559 : 1999 : R2018 Standard Test Method for Volatile Matter in Silicone Fluid (Withdrawn 2022)
ASTM D 2129 : 2005 : R2010 Standard Test Method for Color of Clear Electrical Insulating Liquids (Platinum-Cobalt Scale)
ASTM D 2864 : 2017 : REV A Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 4059 : 2000 : R2005 : EDT 1 Standard Test Method for Analysis of Polychlorinated Biphenyls in Insulating Liquids by Gas Chromatography
ASTM D 1298 : 1999 : R2005 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 4059 : 2000 Standard Test Method for Analysis of Polychlorinated Biphenyls in Insulating Liquids by Gas Chromatography
ASTM D 4052 : 2009 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 5282 : 2005 : R2012 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 4652 : 2005 : R2012 Standard Specification for Silicone Fluid Used for Electrical Insulation
ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 1298 : 2012 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 924 : 2015 : REDLINE Standard Test Method for Dissipation Factor (or Power Factor) and Relative Permittivity (Dielectric Constant) of Electrical Insulating Liquids
ASTM D 4652 : 1992 : R1997 Standard Specification for Silicone Fluid Used for Electrical Insulation
ASTM D 1298 : 1999 : EDT 2 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 1169 : 2002 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 4559 : 1999 : EDT 1 Standard Test Method for Volatile Matter in Silicone Fluid
ASTM D 2129 : 2005 Standard Test Method for Color of Clear Electrical Insulating Liquids (Platinum-Cobalt Scale)
ASTM D 1298 : 1999 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 1816 : 2003 Standard Test Method for Dielectric Breakdown Voltage of Insulating Oils of Petroleum Origin Using VDE Electrodes
ASTM D 2864 : 2006 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 4059 : 2000 : R2010 Standard Test Method for Analysis of Polychlorinated Biphenyls in Insulating Liquids by Gas Chromatography
ASTM D 4052 : 2011 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1481 : 2002 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 1533 : 2000 : R2005 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
ASTM D 4052 : 2016 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 2129 : 2017 : REDLINE Standard Test Method for Color of Clear Electrical <brk/>Insulating Liquids (Platinum-Cobalt Scale)
ASTM D 1533 : 2012 : REDLINE Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
ASTM D 1169 : 2009 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 4559 : 1999 Standard Test Method for Volatile Matter in Silicone Fluid
ASTM D 1816 : 2012(R2019) Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using VDE Electrodes
ASTM D 1807 : 2000 Standard Test Methods for Refractive Index and Specific Optical Dispersion of Electrical Insulating Liquids
ASTM D 2864 : 2010 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 2129 : 2017 Standard Test Method for Color of Clear Electrical <brk/>Insulating Liquids (Platinum-Cobalt Scale)
ASTM D 1298 : 1999 : EDT 1 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 2864 : 2002 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 2864 : 2000 : REV A Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 1169 : 2011 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 1169 : 1995 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 1816 : 2004 Standard Test Method for Dielectric Breakdown Voltage of Insulating Oils of Petroleum Origin Using VDE Electrodes
ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D 5282 : 2005 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 2161 : 1993 : R1999 : EDT 2 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 2864 : 2010 : EDT 1 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 923 : 2015 : REDLINE Standard Practices for Sampling Electrical Insulating Liquids
ASTM D 1169 : 2002 : EDT 1 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 1481 : 2012 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 1807 : 2000 : R2005 Standard Test Methods for Refractive Index and Specific Optical Dispersion of Electrical Insulating Liquids
ASTM D 2161 : 2010 : R2016 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 2161 : 1966 Standard Method Of Test For Conversion Of Kinematic Viscosity To Saybolt Universal Viscosity Or To Saybolt Furol Viscosity
ASTM D 1169 : 2019 Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 2129 : 1997 Standard Test Method for Color of Clear Electrical Insulating Liquids (Platinum-Cobalt Scale)
ASTM D 2864 : 2019 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 2864 : 2007 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 1481 : 2002 : R2007 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 4052 : 2015 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 2161 : 2004 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 1169 : 2019 : REV A Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids
ASTM D 1481 : 2017 : REDLINE Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
ASTM D 2161 : 2017 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 1816 : 1997 Standard Test Method for Dielectric Breakdown Voltage of Insulating Oils of Petroleum Origin Using VDE Electrodes
ASTM D 1533 : 2000 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
ASTM D 4059 : 2000 : R2018 Standard Test Method for Analysis of Polychlorinated Biphenyls in Insulating Liquids by Gas Chromatography
ASTM D 2161 : 2005 : EDT 1 Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity
ASTM D 1816 : 2012 Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using VDE Electrodes
ASTM D 5282 : 1998 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 4052 : 2018 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 4559 : 1999 : R2010 Standard Test Method for Volatile Matter in Silicone Fluid
ASTM D 2864 : 2017 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 1807 : 2000 : R2005 : EDT 1 Standard Test Methods for Refractive Index and Specific Optical Dispersion of Electrical Insulating Liquids (Withdrawn 2014)

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