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ASTM D 500 : 1995 : R2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods of Chemical Analysis of Sulfonated and Sulfated Oils
Available format(s)

Hardcopy , PDF

Superseded date

07-28-2023

Language(s)

English

Published date

08-03-2016

Publisher

American Society for Testing and Materials

CONTAINED IN VOL. 15.04, 2016 Specifies the chemical analysis of sulfonated and sulfated oils.

1.1These test methods cover the chemical analysis of sulfonated and sulfated oils. The analytical procedures appear in the following order:

Section

Moisture:

 Test Method A. Water by Distillation with Volatile Solvent

4 – 9

 Test Method B. Moisture and Volatile Matter by Hot-Plate Method

10 – 14

Organically Combined Sulfuric Anhydride:

 Test Method A. Titration Test

15 – 19

 Test Method B. Extraction-Titration Test

20 – 24

 Test Method C. Ash-Gravimetric Test (in the Presence of True
Sulfonates)

25 – 28

Total Desulfated Fatty Matter

29 – 32

Total Active Ingredients

33 – 36

Unsaponifiable Nonvolatile Matter

37 – 41

Inorganic Salts

42 – 46

Total Alkalinity

47 – 49

Total Ammonia

50 – 52

Acidity as Free Fatty Acids or Acid Number:

 Test Method A. In the Absence of Ammonium or Triethanolamine Soaps

53 – 56

 Test Method B. In the Presence of Dark Colored Oils but in the
Absence of Ammonium or Triethanolamine Soaps (Brine Test)

57 – 60

 Test Method C. In the Presence of Ammonium or Triethanolamine Soaps

61 – 63

Water-Immiscible Organic Solvents Volatile with Steam

64 – 70

1.2The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate.

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.

Committee
D 12
DocumentType
Test Method
Pages
12
ProductNote
Reconfirmed 2016
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 5354 : 1995 : R2020 Standard Test Method for Determination of Total Active Ingredients in Sulfonated and Sulfated Oils
ASTM D 5351 : 1993 : R2021 Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Extraction Titration, Test Method B
ASTM D 5350 : 1995 : R2019 Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Titration, Test Method A
ASTM D 5348 : 1995 : R2019 Standard Test Method for Determination of the Moisture Content of Sulfonated and Sulfated Oils by Distillation with Xylene
ASTM D 5352 : 1995 : R2019 Standard Test Method for Determination of Organically Combined Sulfuric Anhydride Ash-Gravimetric, Test Method C
ASTM D 5349 : 2019 Standard Test Method for Determination of the Moisture and Volatile Content of Sulfonated, Sulfated Oils and Fatliquors by Oven Method
ASTM D 5353 : 1995 : R2019 Standard Test Method for Determination of Total Desulfated Fatty Matter

ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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PDF - English
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