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ASTM D 7439 : 2014 : REDLINE

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass Spectrometry
Available format(s)

PDF

Superseded date

11-11-2021

Language(s)

English

Published date

01-15-2014

CONTAINED IN VOL. 11.07, 2014 Describes a procedure for sample preparation and analysis of airborne particulate matter for the content of metals and metalloids in workplace air samples using inductively coupled plasma-mass spectrometry (ICP-MS).

1.1This standard test method specifies a procedure for sample preparation and analysis of airborne particulate matter for the content of metals and metalloids in workplace air samples using inductively coupled plasma–mass spectrometry (ICP-MS). This test method can be used for other air samples provided the user ensures the validity of the test method (by ensuring that appropriate data quality objectives can be achieved).

1.2This standard test method assumes that samples will have been collected in accordance with Test Method D7035.

1.3This standard test method should be used by analysts experienced in the use of ICP-MS, the interpretation of spectral and matrix interferences and procedures for their correction.

1.4This standard test method specifies a number of alternative methods for preparing test solutions from samples of airborne particulate matter. One of the specified sample preparation methods is applicable to the measurement of soluble metal or metalloid compounds. Other specified methods are applicable to the measurement of total metals and metalloids.

1.5It is the user's responsibility to ensure the validity of the standard method for filters of untested matrices.

1.6Table 1 provides a non-exclusive list of metals and metalloids for which one or more of the sample dissolution methods specified in this document is applicable.

1.7This standard test method is not applicable to compounds of metals and metalloids that are present in the gaseous or vapor state.

1.8No detailed operating instructions are provided because of differences among various makes and models of suitable ICP-MS instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.

1.9The values stated in SI units are to be regarded as standard.

1.10This standard test method contains notes that are explanatory and are not part of the mandatory requirements of the method.

1.11This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 22
DocumentType
Redline
Pages
37
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

ISO 30011:2010 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry
ASTM D 1356 : 2017 : REDLINE Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM E 1583 : 2017 Standard Practice for Evaluating Laboratories Engaged in Determination of Lead in Paint, Dust, Airborne Particulates, and Soil Taken From and Around Buildings and Related Structures
ASTM D 7659 : 2010 : R2015 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
ASTM D 7707 : 2011 : R2016 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
09/30165939 DC : 0 BS ISO 30011 - WORKPLACE AIR - DETERMINATION OF METALS AND METALLOIDS IN AIRBORNE PARTICULATE MATTER BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY
ASTM C 1168 : 2015 : REDLINE Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM D 7035 : 2016 : REDLINE Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
BS ISO 30011:2010 Workplace air. Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry
ASTM D 7659 : 2010 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
ASTM E 1775 : 2016 : REDLINE Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
ASTM D 7707 :2011 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust

ASTM D 7202 : 2015 : REDLINE Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
ASTM E 1613 : 2012 : REDLINE Standard Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES), Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
ISO 3585:1998 Borosilicate glass 3.3 Properties
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 15202-3:2004 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry Part 3: Analysis
ASTM D 6785 : 2013 Standard Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption Spectrometry
ISO 15202-1:2012 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry Part 1: Sampling
ISO 17294-1:2004 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 1: General guidelines
ASTM D 4185 : 2017 : REDLINE Standard Test Method for Measurement of Metals in Workplace Atmospheres by Flame Atomic Absorption Spectrophotometry
ASTM D 7035 : 2016 : REDLINE Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 5011 : 2017 : REDLINE Standard Practices for Calibration of Ozone Monitors Using Transfer Standards
EN 1540:2011 Workplace exposure - Terminology
ISO 17294-2:2016 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 2: Determination of selected elements including uranium isotopes
ISO 15202-2:2012 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry Part 2: Sample preparation

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