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ASTM E 32 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practices for Sampling Ferroalloys and Steel Additives for Determination of Chemical Composition

Available format(s)

Hardcopy , PDF

Superseded date

05-26-2021

Language(s)

English

Published date

02-29-2016

CONTAINED IN VOL. 03.05, 2016 Defines procedures for the sampling of the various ferroalloys and steel additives, either before or after shipment from the plants of the manufacturers.

1.1These practices include procedures for the sampling of the various ferroalloys and steel additives, either before or after shipment from the plants of the manufacturers. They are designed to give results representative of each lot that will be comparable with the manufacturer's guaranteed analysis for the same lot. For check analysis, the purchaser may use any sampling procedure he desires, but the analytical results obtained on such samples shall not be a basis for complaint or rejection, unless the procedure followed is of an accuracy equivalent to that prescribed in these methods.

1.2In sampling ferroalloys and steel additives, serious errors often occur from contamination of the samples by iron from the sampling appliances. Therefore, special precautions should be observed to avoid this source of error. Metallic iron may be removed with a magnet from nonmagnetic alloys; its estimation in other alloys requires special analytical procedures (Note 1). To avoid this error, parts of crushers and pulverizing equipment contacting the samples shall be of steel or other material showing a high resistance to abrasion of the type involved.

Note 1:Metallic iron in ferrochromium and ferrosilicon may be determined as follows: Transfer 5 g of the sample of alloy to a 150-mL beaker, add 25 mL of HNO3 (1 + 3), cover, boil 5 min, filter into a 250-mL beaker, and wash with hot water. Add NH4OH in slight excess, heat to boiling, filter, and wash with hot water. Dissolve the precipitate on the paper with a minimum quantity of hot HCl (1 + 2), wash the filter with hot water, and titrate the iron by a standard procedure such as that described in Test Method E354.

1.3The values stated in SI units are to be regarded as the standard. The inch-pound values in parenthesis are given for information only.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
E 01
DevelopmentNote
Supersedes ASTM A 103. (06/2001)
DocumentType
Standard Practice
Pages
5
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM A 610 : 1979 : R2000 Standard Test Methods for Sampling and Testing Ferroalloys for Determination of Size
ASTM E 362 : 1999 Standard Test Methods for the Determination of Arsenic and Lead in Silicomanganese and Ferrosilicon Manganese (Withdrawn 2005)
ASTM E 364 : 1994 : R2000 Standard Test Methods for Chemical Analysis of Ferrochrome-Silicon (Withdrawn 2006)
ASTM E 371 : 2000 Standard Test Method for the Determination of Boron in Ferroboron (Withdrawn 2006)
ASTM E 2972 : 2015 Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM A 610 : 1979 : R2004 Standard Test Methods for Sampling and Testing Ferroalloys for Determination of Size
ASTM E 360 : 1996 : R2001 Standard Test Methods for Chemical Analysis of Silicon and Ferrosilicon (Withdrawn 2006)
ASTM A 1025 : 2005 : R2010 Standard Specification for Ferroalloys, General Requirements
ASTM E 1724 : 1995 Standard Guide for Testing and Certification of Metal and Metal-Related Reference Materials
ASTM E 31 : 1985 : R1989 Methods for Chemical Analysis of Ferroalloys (Withdrawn 1995)
BS IEC 63004:2015 Standard for receiver fixture interface
ASTM E 361 : 1999 Standard Test Methods for the Determination of Arsenic and Lead in Ferromanganese (Withdrawn 2005)
ASTM E 363 : 2016 : REDLINE Standard Test Methods for Chemical Analysis of Chromium and Ferrochromium
IEC 63004:2015 Standard for receiver fixture interface
ASTM A 1025/A1025M : 2010 Standard Specification for Ferroalloys, General Requirements
ASTM E 1724 : 1995 : R2001 Standard Guide for Testing and Certification of Metal and Metal-Related Reference Materials (Withdrawn 2010)
ASTM E 367 : 2016 Standard Test Methods for Chemical Analysis of Ferroniobium
ASTM A 610 : 1979 : R2014 Standard Test Methods for Sampling and Testing Ferroalloys for Determination of Size
ASTM E 372 : 2013 : REDLINE Standard Test Method for Determination of Calcium and Magnesium in Magnesium Ferrosilicon by EDTA Titration
ASTM E 360 : 1996 Standard Test Methods for Chemical Analysis of Silicon and Ferrosilicon
ASTM A 1025/A1025M : 2010 : R2015 Standard Specification for Ferroalloys and Other Alloying Materials, General Requirements
ASTM E 367 : 2016 : REDLINE Standard Test Methods for Chemical Analysis of Ferroniobium
ASTM A 610 : 1979(R2019) Standard Test Methods for Sampling and Testing Ferroalloys for Determination of Size
ASTM E2972 : 2015(2019) Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 363 : 2016 Standard Test Methods for Chemical Analysis of Chromium and Ferrochromium
ASTM A 1025/A1025M : 2010 : R2020 Standard Specification for Ferroalloys and Other Alloying Materials, General Requirements
ASTM E 372 : 2021 Standard Test Method for Determination of Calcium and Magnesium in Magnesium Ferrosilicon by EDTA Titrimetry
BS 6200-2.2:1993 Sampling and analysis of iron, steel and other ferrous metals. Sampling and sample preparation Methods for ferroalloys and other alloying additives
ASTM A 1025 : 2005 Standard Specification for Ferroalloys, General Requirements
ASTM E 365 : 1999 Standard Test Methods for the Determination of Vanadium in Ferrovanadium and Vanadium Alloying Additives (Withdrawn 2005)
ASTM A 610 : 1979 : R2009 Standard Test Methods for Sampling and Testing Ferroalloys for Determination of Size

ASTM E 354 : 2021 Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys
ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 11 : 2017 : REDLINE Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM E 354 : 2014 Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys
ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 354 : 2014 : REDLINE Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys

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