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BS EN 14185-2:2006

BS EN 14185-2:2006

Current

Current

The latest, up-to-date edition.

Non fatty foods. Determination of N-methylcarbamate residues HPLC method with clean-up on a diatomaceous earth column

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

06-30-2006

Publisher

British Standards Institution

Foreword
1 Scope
2 Principle
3 Reagents
4 Apparatus
5 Sampling
6 Preparation of the samples
7 Procedure
8 Calculation of the results
9 Confirmatory tests
10 Precision, Repeatability and Reproducibility
11 Test report
Annex A (informative) Precision Data
Bibliography

Specifies a high performance liquid chromatographic (HPLC) method for the determination of residues of N-methylcarbamate pesticides in fruits and vegetables and is based on the method of Krause.

This draft European Standard specifies a high performance liquid chromatographic (HPLC) method for the determination of residues of N-methylcarbamate pesticides in fruits and vegetables and is based on the method of Krause [1]. The method has been validated by collaborative study for aldicarb, carbofuran, furathiocarb, methomyl, oxamyl, propoxur and thiodicarb parent compounds and for the metabolites aldicarb sulfoxide, aldicarb sulfone (aldoxycarb) and 3-hydroxy-carbofuran in tomatoes and oranges at levels between 0,04 mg/kg and 0,25 mg/kg. No collaborative data are available for the performance of the method in the determination of other significant compounds although it is known that the method is unsatisfactory for benfuracarb.

Committee
AW/275
DevelopmentNote
Supersedes 04/30124414 DC (06/2006)
DocumentType
Standard
Pages
20
PublisherName
British Standards Institution
Status
Current
Supersedes

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method
ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
ISO 1750:1981 Pesticides and other agrochemicals — Common names

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Hardcopy - English
PDF - English
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