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BS EN ISO 16703:2011

Current
Current

The latest, up-to-date edition.

Soil quality. Determination of content of hydrocarbon in the range C10 to C40 by gas chromatography
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

08-31-2011

Publisher

British Standards Institution

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Interferences
5 Principle
6 Reagents
7 Apparatus
8 Sampling, sample conservation and pretreatment
9 Procedure
10 Precision
11 Test report
Annex A (informative) - Examples of gas chromatograms
        of mineral oil hydrocarbon standard and soil samples
Annex B (informative) - Determination of the boiling range
        of mineral oil hydrocarbons from the gas chromatogram
Annex C (informative) - Precision data
Bibliography

Provides a method for the quantitative determination of the mineral oil (hydrocarbon) content in field-moist soil samples by gas chromatography.

This International Standard specifies a method for the quantitative determination of the mineral oil (hydrocarbon) content in field-moist soil samples by gas chromatography. The method is applicable to mineral oil contents (mass fraction) between 100 mg/kg and 10 000 mg/kg soil, expressed as dry matter, and can be adapted to lower limits of detection. This International Standard is applicable to the determination of all hydrocarbons with a boiling range of 175 °C to 525 °C, of n-alkanes from C10H22 to C40H82, of isoalkanes, cycloalkanes, alkylbenzenes, alkylnaphthalenes and polycyclic aromatic compounds, provided that they are not absorbed on the specified column during the clean-up procedure. This International Standard is not applicable to the quantitative determination of hydrocarbons < C10 originating from gasolines. On the basis of the peak pattern of the gas chromatogram obtained, and of the boiling points of the individual n-alkanes listed in Annex B, the approximate boiling range of the mineral oil and some qualitative information on the composition of the contamination can be obtained.

Committee
EH/4
DevelopmentNote
Supersedes 01/564370 DC. Renumbers and supersedes BS ISO 16703. 2011 version incorporates corrigendum to BS ISO 16703. (08/2011)
DocumentType
Standard
Pages
26
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
EN ISO 16703:2011 Identical
ISO 16703:2004 Identical

ISO 9377-2:2000 Water quality Determination of hydrocarbon oil index Part 2: Method using solvent extraction and gas chromatography
ISO 15009:2016 Soil quality Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons Purge-and-trap method with thermal desorption
ISO 10381-1:2002 Soil quality Sampling Part 1: Guidance on the design of sampling programmes
ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
ISO/TR 11046:1994 Soil quality Determination of mineral oil content Method by infrared spectrometry and gas chromatographic method
PREN 14039 : DRAFT 2000 CHARACTERIZATION OF WASTE - DETERMINATION OF HYDROCARBON CONTENT IN THE RANGE OF C[10]-C[40] BY GAS CHROMATOGRAPHY
ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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