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PD CEN/TS 15968:2010

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Determination of extractable perfluorooctanesulphonate (PFOS) in coated and impregnated solid articles, liquids and fire fighting foams. Method for sampling, extraction and analysis by LCqMS or LC-tandem/MS
Available format(s)

Hardcopy , PDF

Withdrawn date

11-27-2023

Language(s)

English

Published date

01-31-2014

Publisher

British Standards Institution

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle
6 Apparatus and Reagents
7 Sampling
8 Sample pre-treatment
9 Extraction
10 Interference with LC-tandemMS
11 Analysis
12 System suitability test
13 Calculation
14 Expression of results
15 Test report
Annex A (informative) - LC-QMS and LC-TOFMS
Annex B (informative)
Annex C (informative) - Confirmation of compound
        identity by MS methods
Bibliography

Establishes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).

This Technical Specification describes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).

The method is applicable for a concentration range for PFOS in the extract solution of 0,5 μg/l to 50 μg/l.

WARNING ― Persons using this Technical Specification should be familiar with normal laboratory practice. This Technical Specification does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.

IMPORTANT ― It is absolutely essential that tests conducted in accordance with this Technical Specification be carried out by suitably qualified staff.

Committee
TCI/100
DevelopmentNote
Issue Date: 31/01/2014. (02/2014)
DocumentType
Standard
Pages
36
PublisherName
British Standards Institution
Status
Withdrawn

Standards Relationship
CEN/TS 15968:2010 Identical

ISO 15194:2009 In vitro diagnostic medical devices Measurement of quantities in samples of biological origin Requirements for certified reference materials and the content of supporting documentation
ISO 6427:2013 Plastics — Determination of matter extractable by organic solvents (conventional methods)
EN ISO 6427:2014 Plastics - Determination of matter extractable by organic solvents (conventional methods) (ISO 6427:2013)
EN ISO 8130-9:1999 Coating powders - Part 9: Sampling (ISO 8130-9:1992)
ISO 187:1990 Paper, board and pulps — Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples
ISO 25101:2009 Water quality Determination of perfluorooctanesulfonate (PFOS) and perfluorooctanoate (PFOA) Method for unfiltered samples using solid phase extraction and liquid chromatography/mass spectrometry
ISO 9113:1986 Plastics Polypropylene (PP) and propylene-copolymer thermoplastics Determination of isotactic index
EN 20187:1993 Paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples (ISO 187:1990)
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 2419:2012 Leather - Physical and mechanical tests - Sample preparation and conditioning (ISO 2419:2012)
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
ISO 8130-9:1992 Coating powders Part 9: Sampling
ISO 2419:2012 Leather — Physical and mechanical tests — Sample preparation and conditioning
EN 12127:1997 Textiles - Fabrics - Determination of mass per unit area using small samples
EN ISO 15194:2009 In vitro diagnostic medical devices - Measurement of quantities in samples of biological origin - Requirements for certified reference materials and the content of supporting documentation (ISO 15194:2009)

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Hardcopy - English
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