Foodstuffs. Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

08-25-2017

Publisher

British Standards Institution

European foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Standard solution preparation
6 Apparatus
7 Procedure
8 GC-MS analysis
9 Calculating and reporting
10 Test report
11 Precision data
Annex A (informative) - Typical chromatograms
Annex B (informative) - GC-MS troubleshooting
Annex C (informative) - Single laboratory validation
Annex D (informative) - Interlaboratory trial precision data
Bibliography

Defines a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS).

This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS). The method has been single-laboratory validated via the analysis of spiked samples (French fries (uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee), ranging from 30 ?g/kg to 1 500 ?g/kg acrylamide. The results from the single laboratory validation were obtained by a laboratory with significant experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 ?g/kg to 2 000 ?g/kg. Critical points of the method are identified in 7.5 and Clause 8.

Committee	AW/275
DocumentType	Standard
Pages	26
PublisherName	British Standards Institution
Status	Current

Standards	Relationship
CEN/TS 17083:2017	Identical

ISO 1042:1998	Laboratory glassware One-mark volumetric flasks
EN ISO 1042 : 1999	LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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PD CEN/TS 17083:2017

Foodstuffs. Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)

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Abstract

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