DD CEN/TS 15439:2006

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle of the measurement method
    5.1 Introduction
    5.2 Sampling
    5.3 Analysis
6 Reagents
    6.1 Solvent for tar collection and Soxhlet extraction
    6.2 Carrier gas in gas chromatography
    6.3 Calibration standards
7 Equipment
    7.1 Equipment for sampling
    7.2 Equipment for sample pretreatment and analysis
8 Preparation of sampling equipment
    8.1 Preconditioning of filter thimbles
    8.2 Cleaning of equipment
    8.3 Preparation of impinger bottles or Petersen column
    8.4 Sampling train leak test
9 Procedure for sampling
    9.1 Introduction
    9.2 Duration of sampling
    9.3 Sampling procedure
10 Storage of samples
11 Preparation for analysis
    11.1 Introduction
    11.2 Requirements for GC calibration standards and internal
         standards (ISTD)
12 Analysis procedures
    12.1 Soxhlet extraction procedure
    12.2 Combination of solvents
    12.3 Determination of particle mass
    12.4 Determination of gravimetric tar mass
    12.5 Determination of individual tar compounds by GC-MS
         or GC-FID
13 Calculation of GC results
14 Performance characteristics
    14.1 Introduction
    14.2 Performance of the analysis methods (Round Robin tests)
    14.3 Performance of the whole Technical Specification
         (parallel tests)
15 Test report
Annex A (informative) List of most abundant individual organic
                      compounds in biomass gasification product
                      gases
Annex B (normative) List of organic compounds for which
                      precision data have been collected
Annex C (normative) Dimensions of the Petersen column
Annex D (informative) Additional information on Round Robin
                      analysis
Annex E (informative) Additional information on parallel tests
Bibliography