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DEFSTAN 03-4/5(2006) : 2006

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

THE PRE-TREATMENT AND PROTECTION OF STEEL ITEMS OF MAXIMUM TENSILE STRENGTH EXCEEDING 1450 MPA
Available format(s)

Hardcopy , PDF

Superseded date

08-12-2011

Language(s)

English

Published date

01-01-2006

Foreword
0 Introduction
1 Scope
2 Warning
3 Normative References
4 Definitions
   4.2 Baking
   4.3 Categorisation of Steels
   4.4 Design Authority
   4.5 Heat Treatment Times
   4.6 Hydrogen Embrittlement
   4.7 Process Control Schedule
   4.8 Physical Preparation
   4.9 Stress Relief
5 Information to be Supplied by the Purchaser
6 Process Control
7 Recommendations for Design and Manufacture
   7.1 Design Considerations
         7.1.1 Choice of Steel
         7.1.2 Avoidance of Stress Concentrations
         7.1.3 Protective Treatment
   7.2 Type Testing
   7.3 Manufacture
         7.3.1 Machining and Grinding
         7.3.2 Chemical Machining
         7.3.3 Cold Forming
         7.3.4 Surface Rolling
         7.3.5 Protection During Manufacture
         7.3.6 Etch Inspection
8 Physical Preparation
   8.1 Stress Relief
         8.1.1 General
         8.1.2 Standard Procedure
         8.1.3 Stress Relief of Items
                 8.1.3.1 Items not given a Treatment to Introduce
                         Beneficial Compressive Stresses into the
                         Surface
                 8.1.3.2 Items given a Treatment to Introduce
                         Beneficial Compressive Stresses into
                         the Surface
                 8.1.3.3 Springs
   8.2 Mechanical Preparation
                 8.2.1.1 Shot Peening
                 8.2.1.2 Surface Rolling
                 8.2.1.3 Abrasive Blasting
9 Cleaning
   9.2 Category 1451 - 1800 MPa Steels
   9.3 Category 1801 MPa and Greater Steels
10 Protective Treatments
   10.1 Precautions Applicable to all Treatments
   10.2 Cadmium Plating (Def Stan 03-19)
         10.2.1 Preparation
         10.2.2 Choice of Electrolyte
         10.2.3 Baking
         10.2.4 Protection Against Vapour Corrosion
   10.3 Physical Vapour Deposition of Aluminium, Cadmium
         and Titanium Nitride (Def Stan 03 parts 1, 2 and 3)
   10.4 Cadmium Coating by Vacuum Evaporation (DTD 940 Obsolete)
   10.5 Zinc Plating (Def Stan 03-20)
   10.6 Hard Chromium Plating (Def Stan 03-14)
         10.6.1 Preparation
         10.6.3 Post Plating Grinding
   10.7 Nickel Plating for Engineering Purposes
         (Def Stan 03-27)
   10.8 Electroless Nickel Coating of Metals (BS EN ISO 4527)
   10.9 Rhodium Plating (DTD 931 Obsolete)
   10.10 Silver Plating (Def Stan 03-9)
   10.11 Gold Plating (Def Stan 03-17)
   10.12 Sprayed Coatings of Aluminium and Zinc
         (BS EN ISO 2063)
   10.13 Phosphate Treatment (Def Stan 03-11)
   10.14 Paint Applied to Uncoated Steel
   10.15 Processes Permitted but not Recommended
         10.15.1 Tin Plating (BS 1872)
         10.15.2 Copper Plating
   10.16 Processes not Permitted
         10.16.1 Tin-Zinc Alloy Plating
         10.16.2 Sheradizing (BS 4921)
         10.16.3 Hot Dip Galvanizing
   10.17 Re-Processing and Re-Furbishment
11 Inspection and Testing
Annex A - Method for Determining Oxidizable Material in
          Sulfuric Acid
   A.1 Methodology

Sets out the special treatments and precautions that are to be observed when protective and other surface treatments are applied to items, including springs, made from steel of specified maximum tensile strength exceeding 1450 MPa.

DevelopmentNote
Supersedes DEFSTAN 03-4/4(1998) (10/2006)
DocumentType
Standard
Pages
22
PublisherName
UK Ministry of Defence Standards
Status
Superseded
SupersededBy
Supersedes

DEFSTAN 03-9/3(2007) : 2007 ELECTRO-DEPOSITION OF SILVER
DEFSTAN 00-970(PT0)/6(2010) : 2010 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 0: PROCEDURES FOR USE, CONTENT AND DEFINITIONS
DEFSTAN 03-29/4(2008) : 2008 PROTECTION OF METALLIC SPRINGS AGAINST CORROSION
DEFSTAN 03-2/6(2011) : 2011 CLEANING AND PREPARATION OF METAL SURFACES
DEFSTAN 00-970(PT0)/7(2011) : 2011 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 0: PROCEDURES FOR USE, CONTENT AND DEFINITIONS
DEFSTAN 03-36/2(2010) : 2010 GUIDANCE TO THE USE OF CADMIUM ALTERNATIVES IN THE PROTECTIVE COATING OF DEFENCE EQUIPMENT
DEFSTAN 03-28(PT3)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 3: PHYSICAL VAPOUR DEPOSITION OF TITANIUM NITRIDE FOR SURFACE PROTECTION
DEFSTAN 03-28(PT2)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 2: PHYSICAL VAPOUR DEPOSITION OF CADMIUM FOR PROTECTION AGAINST CORROSION
DEFSTAN 03-11/5(2008) : 2008 PHOSPHATE TREATMENT OF IRON AND STEEL
DEFSTAN 03-2/5(2009) : 2009 CLEANING AND PREPARATION OF METAL SURFACES
DEFSTAN 03-28(PT1)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 1: PHYSICAL VAPOUR DEPOSITION OF ALUMINIUM FOR PROTECTION AGAINST CORROSION
DEFSTAN 00-970(PT0)/5(2007) : 2007 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 0: PROCEDURES FOR USE, CONTENT AND DEFINITIONS
DEFSTAN 03-39/1(2008) : 2008 ELECTRODEPOSITION OF ZINC-COBALT ALLOYS
DEFSTAN 03-17/3(2007) : 2007 ELECTRO-DEPOSITION OF GOLD
DEFSTAN 03-19/4(2010) : 2010 ELECTRO-DEPOSITION OF CADMIUM
DEFSTAN 03-43/1(2008) : 2008 THERMAL SPRAYED COATINGS FOR WEAR RESISTANCE
DEFSTAN 03-40/1(2008) : 2008 ELECTRODEPOSITION OF ZINC-NICKEL ALLOYS
DEFSTAN 03-41/1(2008) : 2008 TRIVALENT CHROMIUM PASSIVATION TREATMENTS FOR ELECTRODEPOSITED ZINC-BASE COATINGS

DEFSTAN 03-30/3(2005) : 2005 TREATMENTS FOR THE PROTECTION FOR METAL PARTS OF SERVICE STORES AND EQUIPMENT AGAINST CORROSION
DEFSTAN 80-207/2(2003) : 2003 PAINT, PRIMING, ZINC CHROMATE, NON AIRCRAFT USE, LOW VOC SINGLE OR MULTI-PACK
BS 4921:1988 Specification for sherardized coatings on iron or steel
DEFSTAN 03-27/3(2005) : 2005 ELECTRO-DEPOSITION OF NICKEL FOR ENGINEERING PURPOSES
DEFSTAN 03-19/3(2005) : 2005 ELECTRO-DEPOSITION OF CADMIUM
BS 2X 34:1998 Specification for two component polyurethane finish for aerospace purposes
DEFSTAN 03-11/4(2003) : 2003 PHOSPHATE TREATMENT OF IRON AND STEEL
BS EN 2828:1993 Adhesion test for metallic coatings by burnishing
BS EN ISO 6507-1:2005 Metallic materials. Vickers hardness test Test method
DEFSTAN 03-9/2(1992) : 1992 ELECTRO-DEPOSITION OF SILVER
DTD 931 : AUG 70 RHODIUM PLATING
BS EN 2832:1993 Hydrogen embrittlement of steels. Notched specimen test
DEFSTAN 03-21/3(2002) : 2002 MECHANICAL METHODS FOR THE INDUCEMENT OF RESIDUAL SURFACE COMPRESSIVE STRESSES
BS 7195(1989) : 1989 GUIDE FOR PREVENTION OF CORROSION OF METALS CAUSED BY VAPOURS FROM ORGANIC MATERIALS
DEFSTAN 80-161/1(1995) : 1995 AMD 1 1999 PAINT, SPRAYING, EPOXY, TWO-PACK - TYPES: GLOSS, SEMI-GLOSS, EGG SHELL AND MATT
DTD 940 : NOV 68 THE CADMIUM COATING OF VERY STRONG STEEL PARTS BY VACUUM EVAPORATION
DEFSTAN 80-208/3(2005) : 2005 PAINT FINISHING, POLYURETHANE MULTI-PACK, MATT, IRR, CHEMICAL AGENT RESISTANT, NON AIRCRAFT USE, LOW VOC
BS EN 2829:1995 Adhesion test for metallic coatings by shot peening
BS M 37:1970 Method for the etch inspection of metallic materials and components
BS EN ISO 4527:2003 Metallic coatings. Autocatalytic (electroless) nickel-phosphorus alloy coatings. Specification and test methods
DEFSTAN 03-14/3(2005) : 2005 ELECTRO-DEPOSITION OF CHROMIUM FOR ENGINEERING PURPOSES
DEFSTAN 03-2/4(2005) : 2005 CLEANING AND PREPARATION OF METAL SURFACES
DEFSTAN 03-31/1(1993) : 1993 A GUIDE TO THE USE OF CHROMIUM PLATING FOR ENGINEERING PURPOSES
DEFSTAN 80-54/4(2005) : 2005 PAINT, FINISHING, GENERAL SERVICE, FUEL RESISTANT, GLOSS - TYPE: BRUSHING OR SPRAYING
DEFSTAN 80-206/2(2003) : 2003 PAINT, PRIMING, ZINC PHOSPHATE, NON AIRCRAFT USE, LOW VOC SINGLE OR MULTI-PACK
DEFSTAN 03-17/2(1992) : 1992 ELECTRO - DEPOSITION OF GOLD
BS 2M 54:1991 Specification for temperature control in the heat treatment of metals
DEFSTAN 03-36/1(2005) : 2005 GUIDANCE TO THE USE OF CADMIUM ALTERNATIVES IN THE PROTECTIVE COATING OF DEFENCE EQUIPMENT
BS EN 2831:1993 Hydrogen embrittlement of steels. Test by slow bending
DEFSTAN 91-70/1(1990) : 1990 CUTTING FLUID, SOLUBLE, BIOSTABLE - JOINT SERVICE DESIGNATION ZX-9
DEFSTAN 00-970/1(1983) : 1983 DESIGN REQUIREMENTS FOR SERVICE AIRCRAFT
BS 2X 33:1998 Specification for two component epoxy primer for aerospace purposes
BS EN 2830:1993 Adhesion test for metallic coatings by shearing action
BS EN ISO 2063:2005 Thermal spraying. Metallic and other inorganic coatings. Zinc, aluminium and their alloys
DEFSTAN 03-20/3(2005) : 2005 ELECTRO-DEPOSITION OF ZINC

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