WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2015

Publisher

German Institute for Standardisation (Deutsches Institut für Normung)

National foreword
National Annex NA (informative) - Bibliography
European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Quantification
11 Expression of results
12 Test report
Annex A (informative) - Suitable gas chromatographic
        conditions and example chromatograms
Annex B (informative) - Repeatability and reproducibility
        data
Annex C (informative) - Examples of suitable solid phase
        extraction disks
Annex D (informative) - Clean up procedure
Bibliography

Defines a method for the determination of six selected polybrominated diphenyl ethers (PBDE) listed in Table 1, representative for technical brominated diphenyl ethers (BDE) in water samples in mass concentrations => 0,025 ng/l for each individual congener.

DocumentType	Standard
Pages	35
PublisherName	German Institute for Standardisation (Deutsches Institut für Normung)
Status	Current

Standards	Relationship
EN 16694 : 2015	Identical

DIN ISO 5725-2:2002-12	Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
EN 16377:2013	Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
EN ISO 22032:2009	Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006)
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 22032:2006	Water quality — Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge — Method using extraction and gas chromatography/mass spectrometry
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN ISO 5667-1 : 2006 COR 2007	WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES

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DIN EN 16694 E : 2015

Current

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