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EN 1186-15:2002

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Materials and articles in contact with foodstuffs - Plastics - Part 15: Alternative test methods to migration into fatty food simulants by rapid extraction into iso-octane and/or 95 % ethanol
Withdrawn date

03-31-2003

Published date

09-25-2002

Foreword
1 Scope
2 Normative references
3 Method A Alternative test method to migration into fatty
   food simulants by rapid extraction into iso-octane and/or
   95% ethanol by total immersion
4 Method B Alternative test method to migration into fatty
   food simulants by rapid extraction into iso-octane and/or
   95% ethanol in the single side mode by cell
Annex ZA (informative) Relationship of this European Standard
         with Council Directive 89/109/EEC and Commission
         Directive 90/128/EEC and associated Directives
Bibliography

This European Standard specifies two alternative test methods, in the sense of an extraction test with a 'more severe' test character, for the assessment of the overall migration into fatty food simulants. Method A is based on the determination of the extraction of migrateable substances from plastics which are intended to come into contact with foodstuffs, by total immersion in non-polar, iso-octane, and/or polar, ethanol, solvents depending on the polarity of the packaging material. According to results obtained by this method (see [1],[2],[3],[4],[5],) and taking physio-chemical considerations into account, the obtained extraction efficiency has, generally, been found to be equivalent to or higher than overall migration results obtained under the test conditions, 10 days at 40 °C, 2 h at 70 °C, 1 h at 100 °C, 30 min at 121 °C and 30 min at 130 °C.To ensure as complete as possible extraction of the potential migrants, a strong interaction, e.g. swelling, of the sample by the extraction solvent is necessary. For this purpose, iso-octane is used as an extraction solvent for plastics materials and articles containing non polar food contact layers, such as polyolefins. For test samples made from polar food contact plastics such as polyamide and polyethylene terephthalate, 95 % (v/v) aqueous ethanol is used. For polystyrenes, plasticized polyvinyl chloride and other polymers where the identification or polarity of the polymer is not clear, two parallel extraction tests should be conducted using both of the proposed extraction solvents and taking the higher value obtained as the relevant result.NOTE 1In case of multilayer structures such as plastics laminates and co-extruded plastics, the nature of the food contact layer determines the selection of the extraction solvent(s).

Committee
CEN/TC 194
DevelopmentNote
To be read in conjunction with EN 1186-1. (11/2002)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn

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