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EN 14331:2004

Current
Current

The latest, up-to-date edition.

Liquid petroleum products - Separation and characterisation of fatty acid methyl esters (FAME) from middle distillates - Liquid chromatography (LC)/gas chromatography (GC) method
Published date

03-24-2004

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling
7 Procedure
8 Determination of the composition of a mixture of methyl esters
9 Expression of results
10 Precision
11 Interpretation of results
12 Test report
Annex A (normative) Summary of the conditions for analysis of
        fatty acid methyl esters by gas chromatography
Annex B (informative) Example of a FAME chromatogram
Annex C (informative) Typical compositional data for fatty
        acids in vegetable oils
Bibliography

This European Standard specifies a method for the separation of fatty acid methyl esters (FAME) from middle distillate fuel by liquid chromatography (LC) and for quantitative determination of the individual esters by gas chromatography (GC). This method is applicable to FAME of vegetable or animal origin that contain methyl esters between C14 to C24. These FAME are mainly composed of C16 - C18 fatty acids. This method is applicable whatever the origin of the middle distillate fuel.This test method has been evaluated for the separation and characterisation of FAME present at up to 5 % (V/V) in middle distillate fuel.NOTEFor the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

Committee
CEN/TC 19
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
DIN EN 14331:2004-06 Identical
GOST R EN 14331 : 2010 Identical
NBN EN 14331 : 2004 Identical
NEN EN 14331 : 2004 Identical
NS EN 14331 : 1ED 2004 Identical
I.S. EN 14331:2004 Identical
PN EN 14331 : 2007 Identical
SN EN 14331 : 2005 Identical
UNI EN 14331 : 2005 Identical
UNE-EN 14331:2004 Identical
SS-EN 14331:2004 Identical
BS EN 14331:2004 Identical
NF EN 14331 : 2004 Identical
DIN EN 14331 E : 2004 Identical

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
11/30249539 DC : 0 BS EN 590 - AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
BS EN 590 : 2013 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
I.S. EN 16300:2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
I.S. EN 14213:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
DIN EN 16300:2012-11 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
UNE-EN 16300:2013 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
BS 2000-607(2012) : 2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
PREN 590 : DRAFT 2011 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 15940 E : 2016 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
BS EN 16300:2012 Automotive fuels. Determination of iodine value in fatty acid methyl esters (FAME). Calculation method from gas chromatographic data
11/30245755 DC : 0 BS EN 16300 - AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
UNI EN 16300 : 2013 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
DIN EN 15940:2016-09 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
EN 590:2013 Automotive fuels - Diesel - Requirements and test methods
BS EN 14213:2003 Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods
EN 14213:2003/AC:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
EN 16300:2012 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
I.S. EN 590:2013+A1:2017&LC:2017 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
UNE-EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
DIN EN 14213 E : 2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14213:2003-11 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
EN 14103:2011 Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of ester and linolenic acid methyl ester contents
ISO 5508:1990 Animal and vegetable fats and oils Analysis by gas chromatography of methyl esters of fatty acids
EN ISO 5508 : 1995 ANIMAL AND VEGETABLE FATS AND OILS - ANALYSIS BY GAS CHROMATOGRAPHY OF METHYL ESTERS OF FATTY ACIDS
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)

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