EN 15308:2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
03-12-2022
10-12-2016
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Safety precautions
8 Interferences
9 Sample storage
10 Pretreatment
11 Procedure
12 Calculation
13 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Examples of GC-MS
chromatograms of a calibration standard
solution and a contaminated soil sample
Annex C (informative) - Examples of GC-ECD
chromatograms of a calibration standard
solution and a cable shredder sample
Annex D (normative) - Calculation method for
the estimation of total PCB content
Annex E (informative) - Summary of general
requirements and recommendations
Bibliography
This draft European Standard specifies a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection. The basic content of this standard is identical to that of the Horizontal PCB-standard and is therefore also applicable to soil, sludge and treated bio-waste. The detection and the quantification limits in this method are dependent on sample intake, the level of interferences as well as instrumental limitations. Under the conditions specified in this standard, minimum amounts of individual PCB congeners equal or above 0,01 mg/kg dry matter can typically be determined with no interferences present.NOTEFor the analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to EN 61619, EN 12766–1 and EN ISO 6468 respectively.The method may be applied to the analysis of other PCB congeners not specified in the scope, but its suitability should be proven by proper in-house validation experiments.
| Committee |
CEN/TC 444
|
| DevelopmentNote |
Supersedes PREN 15308. (11/2016)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
| Standards | Relationship |
| NBN EN 15308 : 2008 | Identical |
| DIN EN 15308:2016-12 | Identical |
| UNI EN 15308 : 2008 | Identical |
| PN-EN 15308: 2017-02 | Identical |
| SN EN 15308 : 2016 | Identical |
| NS EN 15308 : 2008 | Identical |
| UNE-EN 15308:2017 | Identical |
| NF EN 15308 : 2017 | Identical |
| BS EN 15308:2016 | Identical |
| I.S. EN 15308:2016 | Identical |
| NEN EN 15308 : 2016 | Identical |
| DIN EN 15308 E : 2016 | Identical |
| PD CLC/TS 50625-3-1:2015 | Collection, logistics & treatment requirements for WEEE Specification for de-pollution. General |
| DIN EN 16167:2012-11 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| 17/30364005 DC : 0 | BS EN 16181 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| BS EN 16167:2012 | Sludge, treated biowaste and soil. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
| UNI EN 16457 : 2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| I.S. EN 16457:2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| 17/30348303 DC : 0 | BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT |
| UNE-EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| S.R. CEN/TS 16181:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| I.S. EN 15002:2015 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| UNI EN 16167 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| UNE-EN 16457:2014 | Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report |
| 12/30231385 DC | BS ISO 13876. Soil quality. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
| ISO 13876:2013 | Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
| UNI CEN/TS 16181 : 2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| S.R. CLC/TS 50625-3-1:2015 | COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL |
| 10/30147454 DC : 0 | BS EN 16167 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| 12/30263896 DC : 0 | BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| DIN EN 16457:2014-07 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| PREN 16167 : DRAFT 2017 | SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| 13/30291099 DC : 0 | BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| ISO 13859:2014 | Soil quality — Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC) |
| 12/30231382 DC : 0 | BS ISO 13859 - SOIL QUALITY - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| DIN EN 15002:2015-07 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN 16457:2014 | Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report |
| CLC/TS 50625-3-1:2015 | Collection, logistics & treatment requirements for WEEE - Part 3-1: Specification for de-pollution - General |
| 17/30364002 DC : 0 | BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| DIN EN 16457 E : 2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| BS EN 16457:2014 | Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report |
| I.S. EN 16167:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD) |
| EN 16167:2012 | Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
| DIN EN 15002 E : 2015 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| 10/30147451 DC : 0 | EN 16181 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) POLYCYCLIC AROMATIC HYDROCARBONS |
| BS EN 15002:2015 | Characterization of waste. Preparation of test portions from the laboratory sample |
| CEN/TS 16181:2013 | Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC) |
| EN ISO 6468 : 1996 | WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION |
| EN 12766-1:2000 | Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD) |
| ISO 11464:2006 | Soil quality Pretreatment of samples for physico-chemical analysis |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| EN 61619:1997 | Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography |
| EN 14346:2006 | CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT |
| ISO 14507:2003 | Soil quality Pretreatment of samples for determination of organic contaminants |
| EN 12766-2:2001 | Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| ISO 6468:1996 | Water quality Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes Gas chromatographic method after liquid-liquid extraction |
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