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EN 15470:2017

Current
Current

The latest, up-to-date edition.

Liquefied petroleum gases - Determination of dissolved residues - High temperature Gas chromatographic method
Published date

07-05-2017

European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calculations
10 Expression of results
11 Precision
Annex A (normative) - Equipment for sample transfer
        and evaporation
Annex B (informative) - Examples of gas chromatograms
Bibliography

This European Standard specifies a method for determining the dissolved residual matter in liquefied petroleum gases (LPG), in the range of 40 mg/kg to 100 mg/kg. Higher concentrations can be determined by adjusting the sample size.The dissolved residue is the amount of organic compounds that are detectable by gas chromatography after evaporation of the sample at ambient temperature and then in an oven at 105 °C.This method is not suitable for detecting solid materials or for possibly high molar mass polymers (>1 000 g/mol).From the analysis of a limited LPG sample size (50 g to 75 g) this method allows obtaining information on the potential origin of the residue (gasoil, lubricants, plasticizers, etc.).The precision data of the method have been determined from 20 mg/kg to 100 mg/kg. For a higher content of residue, the precision has not been tested.NOTEAn alternative European Standard, EN 1547113[1], specifies a gravimetric method.WARNING - The use of this Standard can involve hazardous materials, operations and equipment. This Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.

DevelopmentNote
Supersedes PREN 15470. (07/2017)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

Standards Relationship
UNI EN 15470:2017 Identical
NF EN 15470 : 2008 Identical
UNE-EN 15470:2017 Identical
NS EN 15470 : 2017 Identical
DIN EN 15470:2016-01 (Draft) Identical
UNI EN 15470 : 2008 Identical
I.S. EN 15470:2017 Identical
NBN EN 15470 : 2008 Identical
PN EN 15470 : 2017 Identical
UNE-EN 15470:2008 Identical
BS EN 15470:2017 Identical
NEN EN 15470 : 2017 Identical
SN EN 15470:2017 Identical
DIN EN 15470 E : 2017 Identical
DIN EN 15470:2017-09 Identical

I.S. EN 589:2008 AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS
12/30263426 DC : 0 BS EN 16423 - LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION
DIN EN 16423:2014-02 Liquefied petroleum gases - Determination of dissolved residue - Gas chromatographic method using liquid, on-column injection
UNE-EN 15471:2017 Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method
BS EN 589 : 2008 AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS
BS EN 16423:2013 Liquefied petroleum gases. Determination of dissolved residue. Gas chromatographic method using liquid, on-column injection
UNI EN 16423 : 2013 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION
15/30330673 DC : 0 BS EN 15471 - LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD
BS ISO 9162:2013 Petroleum products. Fuels (class F). Liquefied petroleum gases. Specifications
DIN EN 589:2012-06 AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS
DIN EN 15471 E : 2017 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD
DIN EN 15471:2016-01 (Draft) LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD
UNE-EN 589:2009 Automotive fuels - LPG - Requirements and test methods
EN 589:2008+A1:2012 Automotive fuels - LPG - Requirements and test methods
PREN 15471 : DRAFT 2015 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD
DIN EN 16423 E : 2014 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION
ISO 9162:2013 Petroleum products — Fuels (class F) — Liquefied petroleum gases — Specifications
UNI EN 589 : 2013 AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS
BS EN 15471:2017 Liquefied petroleum gases. Determination of dissolved residues. High-temperature gravimetric method
EN 16423:2013 Liquefied petroleum gases - Determination of dissolved residue - Gas chromatographic method using liquid, on-column injection
EN 15471:2017 Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method
I.S. EN 15471:2017 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD
12/30261063 DC : 0 BS ISO 9162 - PETROLEUM PRODUCTS - FUELS (CLASS F) - LIQUEFIED PETROLEUM GASES - SPECIFICATIONS
I.S. EN 16423:2013 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION
16/30347787 DC : 0 BS EN 589 - AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS
DIN EN 15471:2017-09 LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD

EN ISO 4257:2001 Liquefied petroleum gases - Method of sampling (ISO 4257:2001)
ISO 4257:2001 Liquefied petroleum gases Method of sampling
EN 15471:2017 Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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