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EN ISO 22032:2009

Current
Current

The latest, up-to-date edition.

Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006)
Published date

02-25-2009

Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
        in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
        electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography

ISO 22032:2006 specifies a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode. When using GC-EI-MS, the method is applicable to samples containing 0,05 to 25 micrograms per kilogram of tetra- to octabromo congeners and 0,3 to 100 micrograms per kilogram of decabromo diphenyl ether (BDE-209), respectively.

Committee
CEN/TC 230
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

DIN EN 16694 E : 2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
DIN EN 16694:2015-12 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
UNE-EN 16694:2016 Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS)
CEN/TR 16417:2016 FOOTWEAR - FOOTWEAR INDUSTRY GUIDELINE FOR SUBSTANCES OF VERY HIGH CONCERN (ANNEX 14 OF REACH)
13/30291096 DC : 0 BS EN 16694 - WATER QUALITY - DETERMINATION OF PENTABROMODIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
UNE-EN 16377:2014 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
S.R. CEN/TR 16417:2016 FOOTWEAR - FOOTWEAR INDUSTRY GUIDELINE FOR SUBSTANCES OF VERY HIGH CONCERN (ANNEX 14 OF REACH)
BS EN 16377:2013 Characterization of waste. Determination of brominated flame retardants (BFR) in solid waste
DIN EN 16377:2013-12 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
PD CEN/TR 16417:2016 Footwear. Footwear industry guideline for substances of very high concern (Annex XIV of REACH)
UNI EN 16377 : 2014 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
EN 16694 : 2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
EN 16377:2013 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
DIN EN 16377 E : 2013 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
BS EN 16694:2015 Water quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS)
I.S. EN 16694:2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
12/30255723 DC : 0 BS EN 16377 - CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
I.S. EN 16377:2013 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE

ISO 5667-13:2011 Water quality Sampling Part 13: Guidance on sampling of sludges
ISO/TR 13530:1997 Water quality Guide to analytical quality control for water analysis
EN 12880:2000 Characterization of sludges - Determination of dry residue and water content
DIN 32645:2008-11 CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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