ISO 6145-4:2004
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Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 4: Continuous syringe injection method
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Language(s)
English, French
Published date
06-15-2004
ISO 6145-4:2004 specifies a method for continuous production of calibration gas mixtures, containing two or more components, from pure gases or other gas mixtures by continuous injection of the calibration component(s) into a complementary gas stream by means of a syringe.
If pre-mixed gases are used instead of pure gases (see Annex A), much lower volume fractions can be obtained. The volume flow rates, from which the volume fractions are determined, can be calculated from the individual flow rates and can be independently measured by a suitable method given in ISO 6145-1.
The merits of the method are that a substantial quantity of the gas mixture can be prepared on a continuous basis and that multi-component mixtures can be prepared almost as readily as binary mixtures if the appropriate number of syringes is utilized, or if the syringe already contains a multi-component mixture of known composition. This method also provides a convenient means for increasing the volume fraction of the calibration component in the mixture in small steps. It is therefore a useful method for evaluation of other characteristics of gas analysers, such as minimum detection limit and dead zone, as well as accuracy. The relative expanded uncertainty in the volume fraction obtainable for a binary mixture (at a coverage factor of 2) is 5 % and the range of applicability is 10-5 to 10-2.
| DevelopmentNote |
Supersedes ISO/DIS 6145-4 (06/2004)
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| DocumentType |
Standard
|
| Pages |
15
|
| PublisherName |
International Organization for Standardization
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| Status |
Current
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| Supersedes |
| Standards | Relationship |
| NBN EN ISO 6145-4 : 2009 | Identical |
| NF EN ISO 6145-4 : 2008 | Identical |
| NEN EN ISO 6145-4 : 2008 | Identical |
| NEN ISO 6145-4 : 2004 | Identical |
| NS EN ISO 6145-4 : 1ED 2008 | Identical |
| I.S. EN ISO 6145-4:2008 | Identical |
| PN EN ISO 6145-4 : 2008 | Identical |
| SAC GB/T 5275-4 : 2014 | Identical |
| SN EN ISO 6145-4:2008 | Identical |
| UNI EN ISO 6145-4 : 2009 | Identical |
| UNE-EN ISO 6145-4:2008 | Identical |
| BIS IS 16249-4 : 2014 | Identical |
| BS ISO 6145-4 : 2004 | Identical |
| BS EN ISO 6145-4:2008 | Identical |
| UNE-ISO 6145-4:2008 | Identical |
| EN ISO 6145-4:2008 | Identical |
| DIN EN ISO 6145-4:2008-11 | Identical |
| UNE 77243-4:2001 | Identical |
| NF ISO 6145-4 : 1986 | Identical |
| BS 4559-5.4:1987 | Identical |
| BS EN 50054:1999 | Electrical apparatus for the detection and measurement of combustible gases. General requirements and test methods |
| BS ISO 14965:2000 | Ambient air. Determination of total non-methane organic compounds. Cryogenic preconcentration and direct flame ionization detection method |
| DIN EN ISO 17621 E : 2015 | WORKPLACE ATMOSPHERES - SHORT TERM DETECTOR TUBE MEASUREMENT SYSTEMS - REQUIREMENTS AND TEST METHODS (ISO 17621:2015) |
| DIN EN ISO 6145-1:2008-11 | GAS ANALYSIS - PREPARATION OF CALIBRATION GAS MIXTURES USING DYNAMIC VOLUMETRIC METHODS - PART 1: METHODS OF CALIBRATION |
| I.S. EN 61779-1:2003 | ELECTRICAL APPARATUS FOR THE DETECTION AND MEASUREMENT OF FLAMMABLE GASES - PART 1: GENERAL REQUIREMENTS AND TEST METHODS |
| BS EN 13528-3:2003 | Ambient air quality. Diffusive samplers for the determination of concentrations of gases and vapours. Requirements and test methods Guide to selection, use and maintenance |
| BS EN ISO 14111:1999 | Natural gas. Guidelines to traceability in analysis |
| BS EN 1231:1997 | Workplace atmospheres. Short term detector tube measurement systems. Requirements and test methods |
| I.S. EN 838:2010 | WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING DIFFUSIVE SAMPLERS - REQUIREMENTS AND TEST METHODS |
| EN 1231:1996 | Workplace atmospheres - Short term detector tube measurement systems - Requirements and test methods |
| EN 1076:2009 | Workplace exposure - Procedures for measuring gases and vapours using pumped samplers - Requirements and test methods |
| EN 13528-3:2003 | Ambient air quality - Diffusive samplers for the determination of concentrations of gases and vapours - Requirements and test methods - Part 3: Guide to selection, use and maintenance |
| EN 50054:1998 | Electrical apparatus for the detection and measurement of combustible gases - General requirements and test methods |
| UNI EN ISO 6145-1 : 2009 | GAS ANALYSIS - PREPARATION OF CALIBRATION GAS MIXTURES USING DYNAMIC VOLUMETRIC METHODS - PART 1: METHODS OF CALIBRATION |
| EN 60079-29-1:2016 | Explosive atmospheres - Part 29-1: Gas detectors - Performance requirements of detectors for flammable gases |
| ISO 10498:2004 | Ambient air — Determination of sulfur dioxide — Ultraviolet fluorescence method |
| 14/30254778 DC : 0 | BS EN ISO 17621 - WORKPLACE ATMOSPHERES - SHORT TERM DETECTOR TUBE MEASUREMENT SYSTEMS - REQUIREMENTS AND TEST METHODS |
| ISA 12.13.01 : 2003 | PERFORMANCE REQUIREMENTS FOR COMBUSTIBLE GAS DETECTORS |
| BS 4559-5.1:1987 | Methods for preparation of calibration gas mixtures. Dynamic volumetric methods Review of methods of calibration |
| UNE-EN 60079-29-1:2017 | Explosive atmospheres - Part 29-1: Gas detectors - Performance requirements of detectors for flammable gases |
| PREN 14662-3 : DRAFT 2013 | AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF BENZENE CONCENTRATIONS - PART 3: AUTOMATED PUMPED SAMPLING WITH IN SITU GAS CHROMATOGRAPHY |
| DIN EN ISO 16017-2:2003-09 | INDOOR, AMBIENT AND WORKPLACE AIR - SAMPLING AND ANALYSIS OF VOLATILE ORGANIC COMPOUNDS BY SORBENT TUBE/THERMAL DESORPTION/CAPILLARY GAS CHROMATOGRAPHY - PART 2: DIFFUSIVE SAMPLING |
| DIN EN 1076:2010-04 | Workplace exposure - Procedures for measuring gases and vapours using pumped samplers - Requirements and test methods |
| DIN EN 14662-3:2016-02 | AMBIENT AIR - STANDARD METHOD FOR THE MEASUREMENT OF BENZENE CONCENTRATIONS - PART 3: AUTOMATED PUMPED SAMPLING WITH IN SITU GAS CHROMATOGRAPHY |
| UNE-EN 14662-3:2016 | Ambient air - Standard method for the measurement of benzene concentrations - Part 3: Automated pumped sampling with in situ gas chromatography |
| IEC 61779-1:1998 | Electrical apparatus for the detection and measurement of flammable gases - Part 1: General requirements and test methods |
| I.S. EN 14042:2003 | WORKPLACE ATMOSPHERES - GUIDE FOR THE APPLICATION AND USE OF PROCEDURES FOR THE ASSESSMENT OF EXPOSURE TO CHEMICAL AND BIOLOGICAL AGENTS |
| I.S. EN 14662-3:2015 | AMBIENT AIR - STANDARD METHOD FOR THE MEASUREMENT OF BENZENE CONCENTRATIONS - PART 3: AUTOMATED PUMPED SAMPLING WITH IN SITU GAS CHROMATOGRAPHY |
| VDI 2100 Blatt 3:2011-10 | Determination of gaseous compounds in ambient air - Determination of indoor air pollutants - Gas chromatographic determination of organic compounds - Active sampling by accumulation on adsorbents - Thermal desorption |
| DIN EN 61779-1 : 2001 AMD 11 2004 | ELECTRICAL APPARATUS FOR THE DETECTION AND MEASUREMENT OF FLAMMABLE GASES - PART 1: GENERAL REQUIREMENTS AND TEST METHODS |
| 13/30272419 DC : 0 | BS EN 14662-3 - AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF BENZENE CONCENTRATIONS - PART 3: AUTOMATED PUMPED SAMPLING WITH IN SITU GAS CHROMATOGRAPHY |
| 08/30163829 DC : DRAFT JAN 2008 | BS EN 1076 - WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING PUMPED SAMPLERS - REQUIREMENTS AND TEST METHODS |
| 08/30172873 DC : DRAFT JULY 2008 | BS EN 838 - WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING DIFFUSIVE SAMPLERS - REQUIREMENTS AND TEST METHODS |
| UNE-EN ISO 17621:2016 | Workplace atmospheres - Short term detector tube measurement systems - Requirements and test methods (ISO 17621:2015) |
| 04/30112677 DC : 0 | IEC 61779-1 ED.2 - ELECTRICAL APPARATUS FOR THE DETECTION AND MEASUREMENT OF FLAMMABLE GASES - PART 1: GENERAL REQUIREMENTS AND TEST METHODS |
| DIN EN ISO 17621:2015-12 | WORKPLACE ATMOSPHERES - SHORT TERM DETECTOR TUBE MEASUREMENT SYSTEMS - REQUIREMENTS AND TEST METHODS (ISO 17621:2015) |
| BS EN 60079-29-1:2007 | Explosive atmospheres Gas detectors. Performance requirements of detectors for flammable gases |
| I.S. EN ISO 17621:2015 | WORKPLACE ATMOSPHERES - SHORT TERM DETECTOR TUBE MEASUREMENT SYSTEMS - REQUIREMENTS AND TEST METHODS (ISO 17621:2015) |
| ISO/TS 14167:2003 | Gas analysis General quality assurance aspects in the use of calibration gas mixtures - Guidelines |
| BS EN 1076:2009 | Workplace exposure. Procedures for measuring gases and vapours using pumped samplers. Requirements and test methods |
| ISO 6145-1:2003 | Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 1: Methods of calibration |
| EN 14662-3:2015 | Ambient air - Standard method for the measurement of benzene concentrations - Part 3: Automated pumped sampling with in situ gas chromatography |
| UNI EN 838 : 2010 | WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING DIFFUSIVE SAMPLERS - REQUIREMENTS AND TEST METHODS |
| 17/30321967 DC : 0 | BS ISO/IEC 20435-1 - WORKPLACE ATMOSPHERES - PART 1: GAS DETECTORS - PERFORMANCE REQUIREMENTS OF DETECTORS FOR TOXIC GASES |
| 17/30345272 DC : 0 | BS ISO 14167 - GAS ANALYSIS - GENERAL QUALITY ASPECTS AND METROLOGICAL TRACEABILITY OF CALIBRATION GAS MIXTURES |
| BS EN ISO 17621:2015 | Workplace atmospheres. Short term detector tube measurement systems. Requirements and test methods |
| NF EN 61779-1 : 2005 AMD 11 2005 | ELECTRICAL APPARATUS FOR THE DETECTION AND MEASUREMENT OF FLAMMABLE GASES - PART 1: GENERAL REQUIREMENTS AND TEST METHODS |
| BS EN ISO 6145-1:2008 | Gas analysis. Preparation of calibration gas mixtures using dynamic volumetric methods Methods of calibration |
| ISO 14965:2000 | Air quality — Determination of total non-methane organic compounds — Cryogenic preconcentration and direct flame ionization detection method |
| DIN EN 838:2010-05 | Workplace exposure - Procedures for measuring gases and vapours using diffusive samplers - Requirements and test methods |
| BS EN ISO 16017-1:2001 | Indoor, ambient and workplace air. Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography Pumped sampling |
| BS EN 14042:2003 | Workplace atmospheres. Guide for the application and use of procedures for the assessment of exposure to chemical and biological agents |
| BS EN 14662-3:2015 | Ambient air. Standard method for the measurement of benzene concentrations Automated pumped sampling with in situ gas chromatography |
| ISO 16017-1:2000 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling |
| ISO 17621:2015 | Workplace atmospheres Short term detector tube measurement systems Requirements and test methods |
| BS EN ISO 16017-2:2003 | Indoor, ambient and workplace air. Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography Diffusive sampling |
| BS EN 838:2010 | Workplace exposure. Procedures for measuring gases and vapours using diffusive samplers. Requirements and test methods |
| I.S. EN 1076:2009 | WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING PUMPED SAMPLERS - REQUIREMENTS AND TEST METHODS |
| EN ISO 6145-1:2008 | Gas analysis - Preparation of calibration gas mixtures using dynamic volumetric methods - Part 1: Methods of calibration (ISO 6145-1:2003) |
| EN ISO 16017-2:2003 | Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 2: Diffusive sampling (ISO 16017-2:2003) |
| EN ISO 16017-1:2000 | Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 1: Pumped sampling (ISO 16017-1:2000) |
| EN 14042:2003 | Workplace atmospheres - Guide for the application and use of procedures for the assessment of exposure to chemical and biological agents |
| EN 838:2010 | Workplace exposure - Procedures for measuring gases and vapours using diffusive samplers - Requirements and test methods |
| I.S. EN 1231:1997 | WORKPLACE ATMOSPHERES - SHORT TERM DETECTOR TUBE MEASUREMENT SYSTEMS - REQUIREMENTS AND TEST METHODS |
| 13/30267536 DC : 0 | BS EN 60079-29-1 ED 2.0 - EXPLOSIVE ATMOSPHERES - PART 29-1: GAS DETECTORS - PERFORMANCE REQUIREMENTS OF DETECTORS FOR FLAMMABLE GASES |
| BS ISO 6145-1 : 2003 | GAS ANALYSIS - PREPARATION OF CALIBRATION GAS MIXTURES USING DYNAMIC VOLUMETRIC METHODS - PART 1: METHODS OF CALIBRATION |
| 17/30323887 DC : 0 | BS EN 62990-131 - WORKPLACE ATMOSPHERES - PART 1: GAS DETECTORS - PERFORMANCE REQUIREMENTS OF DETECTORS FOR TOXIC GASES |
| BS EN 61779-1:2000 | Electrical apparatus for the detection and measurement of flammable gases General requirements and test methods |
| CSA C22.2 NO. 60079-29-1:17 | EXPLOSIVE ATMOSPHERES - PART 29-1: GAS DETECTORS - PERFORMANCE REQUIREMENTS OF DETECTORS FOR FLAMMABLE GASES |
| I.S. EN 60079-29-1:2016 | EXPLOSIVE ATMOSPHERES - PART 29-1: GAS DETECTORS - PERFORMANCE REQUIREMENTS OF DETECTORS FOR FLAMMABLE GASES |
| I.S. EN ISO 6145-1:2008 | GAS ANALYSIS - PREPARATION OF CALIBRATION GAS MIXTURES USING DYNAMIC VOLUMETRIC METHODS - PART 1: METHODS OF CALIBRATION |
| ISO 16017-2:2003 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 2: Diffusive sampling |
| EN 61779-1 : 2000 AMD 11 2004 | ELECTRICAL APPARATUS FOR THE DETECTION AND MEASUREMENT OF FLAMMABLE GASES - PART 1: GENERAL REQUIREMENTS AND TEST METHODS |
| DIN EN 13528-3:2004-04 | Ambient air quality - Diffuse samplers for the determination of concentrations of gases and vapours - Part 3: Guide to selection, use and maintenance |
| EN ISO 17621:2015 | Workplace atmospheres - Short term detector tube measurement systems - Requirements and test methods (ISO 17621:2015) |
| DIN EN 14042:2003-07 | WORKPLACE ATMOSPHERES - GUIDE FOR THE APPLICATION AND USE OF PROCEDURES FOR THE ASSESSMENT OF EXPOSURE TO CHEMICAL AND BIOLOGICAL AGENTS |
| ISO/IEC Guide 98:1993 | Guide to the expression of uncertainty in measurement (GUM) |
| ISO 6145-7:2009 | Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 7: Thermal mass-flow controllers |
| ISO 6143:2001 | Gas analysis — Comparison methods for determining and checking the composition of calibration gas mixtures |
| ISO 7504:2015 | Gas analysis Vocabulary |
| ISO 6145-1:2003 | Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 1: Methods of calibration |
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